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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Advanced Real Time Imaging
Presentation Title On the solid state dendritic growth of carbide at interfaces in a high temperature alloy
Author(s) Yuanbo Tang, Anh Hoang Pham
On-Site Speaker (Planned) Yuanbo Tang
Abstract Scope Solid-state growth of M7C3 carbide at different interfaces in an austenitic Ni–Cr–Fe alloy was studied in-situ by high temperature confocal laser scanning microscopy during continuous cooling from 1140 °C. The carbide develops a dendritic morphology and grows laterally across the free surface via a diffusion-assisted mechanism. Primary dendrite arms can extend beyond 100 microns, with some dendrites also developing secondary arms with spacing approximately 3.0 microns. By using focused ion beam tomography, some of the surface carbides are found to be directly connected to dendritic carbide at grain boundaries in the bulk confirming they originated from the same nucleus. Matrix deformation is induced in the vicinity of a carbide during growth. This work provides significant insight into the important topic of carbide development by a rare combination of both in-situ microscopy and a 3D tomographic technique; the new knowledge discovered is expected to apply to other austenitic systems.
Proceedings Inclusion? Planned:
Keywords High-Temperature Materials, Phase Transformations, Nuclear Materials

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In situ Synthesis and 3D Visualization of Hierarchically-Assembled ZnS Nanostructures
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On the solid state dendritic growth of carbide at interfaces in a high temperature alloy
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