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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Advanced Real Time Imaging
Presentation Title In situ Synthesis and 3D Visualization of Hierarchically-Assembled ZnS Nanostructures
Author(s) Yu-Jin Song, Taehwan Lim, Hee-Suk Chung, JUNG HAN KIM
On-Site Speaker (Planned) Yu-Jin Song
Abstract Scope Nanomaterials have garnered significant interest in enhancing the performance of energy harvesting systems, biomedical devices, and high-strength composites. Despite advances in fabricating elaborate and heterogeneous nanostructures, and characterizing them using TEM tomography, challenges still remain in achieving straightforward 3D visualization, due to complex fabrication processes, agglomeration issues, and non-uniform outputs. Here, we propose an in situ synthesis approach for fabricating complex, hierarchically-assembled ZnS nanostructures which comprise nanowire cores and nanoparticles catalyzed by Ag2S.This study marks the first successful synthesis of a heterogeneous nanostructure, utilizing the phase transformation mechanisms of vapor-liquid-solid for nanowires and vapor-solid for nanoparticles through precise temperature control. The resulting hierarchically-assembled ZnS nanostructures were characterized and their growth mechanisms were elucidated using the advanced TEM techniques. The electron tomography and 3D printing techniques allowed visualization of the nanostructures. This collaborative work is expected to open avenues for fabricating advanced and sophisticated nanostructures with potential applications in diverse fields.
Proceedings Inclusion? Planned:
Keywords Characterization, Nanotechnology, Thin Films and Interfaces

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Accelerating Plasma and Radiation Surface Science Using Transient Grating Spectroscopy
Beam Control in LPBF and High-Speed Visualization
Dissolution of calcium aluminate inclusions in CaO-SiO2-Al2O3 steelmaking slags: an in-situ and modelling study
Exploring the applications of contact-mode high-speed AFM
Improving sub-microsecond x-ray radiography at CHESS
In situ observations of the interfacial phenomenon and non-metallic inclusion behaviors in high-entropy materials by second synthesis
In situ Synthesis and 3D Visualization of Hierarchically-Assembled ZnS Nanostructures
Microparticle impact and ignition in high-pressure oxygen
On the solid state dendritic growth of carbide at interfaces in a high temperature alloy
Operando study of the exfoliation dynamics of 2D materials by X-ray free electron laser MHz imaging and multiphysics modelling
Operando X-ray imaging of solute redistribution in functionally graded materials
Real-Time Imaging and Analysis of Electroconvection Using Advanced Fluorescence Microscopy and Cloud Algorithms
Real-time optical visualization of battery reactions and processes
Real-Time XFEL MHz X-ray Microscopy Study of the Cavitation Dynamics of Highly Viscous Fluids Under Ultrasound
Revealing Weld Bead Dynamics: High-Speed Imaging of Wire Arc DED Process
Study of Cracking Initiation and Evolution Dynamics with In-situ X-ray Imaging and Automated Machine Learning
Time-Resolve X-ray Imaging of Freeze-Thaw Damage in AA7075
Ultra-High Strain Rate Impact Response of Polyethylene at Critical Transition Temperatures
Using Lock-in Thermography to Rapidly Screening Thermal Property of Additive Manufacturing Components
Visualizing localized electrochemical corrosion on metal surfaces using scanning electrochemical cell impedance microscopy

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