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Meeting 2024 TMS Annual Meeting & Exhibition
Symposium Additive Manufacturing: Advanced Characterization with Synchrotron, Neutron, and In Situ Laboratory-scale Techniques III
Presentation Title Improving Porosity Characterization and Analysis in Additive Manufacturing Through 3D X-ray Microscopy Coupled with Deep Learning-based Resolution Recovery
Author(s) Nathan Johnson, Hrishi Bale, Yulia Trenikhina, Stephen Kelly
On-Site Speaker (Planned) Hrishi Bale
Abstract Scope The ultimate performance of the parts produced by metal powder-bed fusion additive manufacturing (AM) processes is dominated by porosity and flaws that emerge in the production process making it is critical to study their effects on the physical and mechanical properties of the produced parts. Laboratory X-ray microscopes enable access to higher resolution 3D imaging through the use of two-stage objective-based magnification approaching sub-micron resolutions. However, the age-old resolution vs field-of-view challenge makes it harder to fully characterize sufficiently large representative volumes in AM, especially in parts with widely distributed pore sizes ranging from nm-to-sub mm and in-homogenously distributed over a large volume. Latest advances in deep-learning based 3D image reconstruction and imaging optics enable mapping porosity at high resolution and over large area using the concept of resolution recovery. We present results demonstrating improvements in pore analysis by combining software and hardware solutions for characterizing complex AM architectures.
Proceedings Inclusion? Planned:
Keywords Characterization, Additive Manufacturing, Machine Learning

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Suite of High-energy Synchrotron Tools for Studies of Additive Manufacturing from Processing to Performance
AI-powered In-situ Pore Generation and Evolution Dynamics for Laser Powder Bed Fusion Process
Alloy Design for Additive Manufacturing
An Electron Beam Melting System for In-situ Synchrotron X-ray Monitoring
An Update on High-Speed Visualization and Beam Control
Characterizing the Effects of Varying Process Parameters on Additive Manufactured Materials for Nuclear Structural Material Applications
Continuous-wave Lasering Improves Strength-Ductility Tradeoff and Fatigue Response of Additively Manufactured Stainless Steels
Controlling Bubble Dynamics Mechanisms during Directed Energy Deposition Additive Manufacturing
Controlling Melt Pool Dynamics during Additive Manufacturing Using External Forces
Controlling Microstructure of Additively Manufactured Ti-6Al-4V through In-situ Selective Laser Heat Treatment
Creep Behavior of an Additively Manufactured Al-Ce-Ni-Mn-Zr Alloy Measured via In Situ Neutron Diffraction
Do Dislocation Structures Evolve during Metal 3D Printing After Solidification? – An In Situ Synchrotron X-ray Diffraction Study
Effect of Ultrasound Melt Treatment in Additive Manufacturing Environment: An In Situ Synchrotron X-ray Diffraction Analysis
Enabling Real-time Characterization of Laser-based Additive Manufacturing through Operando Techniques
Enhancing Mass Transfer in LPBF: A Dive into Oscillating Laser Scan Strategies and Melt Pool Dynamics
F-21: Characterization Using Nano-holotomography of the Healability of a New High Strength Healable AlMg Alloy Produced by Additive Manufacturing
F-23: Examining Process Parameter Effect on Defects in Direct Energy Deposited Stainless Steel 316 Using X-ray Computed Tomography
F-24: From Part Geometry to Melt Pool Geometry: Scan Strategies to Predict and Prevent Defects
F-25: In-situ Acoustic Emission Process Monitoring for Powder-blown Laser Directed Energy Deposition o fRefractory Alloys
F-27: Machine Learning-aided Laser Absorptance Prediction and Keyhole Feature Simulation in Laser Powder Bed Fusion
F-28: Phase Evolution during Multi-material Laser Powder-Bed Fusion via Operando Synchrotron X-ray Diffraction and Imaging
High-energy X-ray Capabilities at APS for Additive Manufacturing Research
How Accurately Can One Determine Temperature and Heating/Cooling Rates from Time-resolved Synchrotron Diffraction Experiments during AM?
Improving Porosity Characterization and Analysis in Additive Manufacturing Through 3D X-ray Microscopy Coupled with Deep Learning-based Resolution Recovery
Improving the Efficiency of Stress-strain Neutron Diffraction Using a Polychromatic Beam and Multiplexing
In-situ Characterisation of Directed Energy Deposition of Selected Nickel Superalloys
In-situ Characterization of Phase Transformation Dynamics in Metal Additive Manufacturing Processes
In-situ Laser Powder Bed Fusion of High Entropy Alloys Analyzed by Synchrotron X-ray Diffraction
In-situ Melt Pool Monitoring Using Synchrotron X-ray Imaging and Ultrasound for Laser-based Additive Manufacturing
In-situ Monitoring of Particle Impact on Melt Pool Flow in Laser Directed Energy Deposition Additive Manufacturing
In-situ Neutron Diffraction Measurements on Electron Beam Additively Manufactured (EBAM) 316 Stainless Steel
In-situ Neutron Studies on Metallic Materials during Laser Powder Bed Fusion
In-situ Study on Fracture Behavior of Friction Stir Deposited AA 6061
In situ Monitoring and Closed-loop Control of Laser, Powder Blown Directed Energy Deposition Using a Coaxial Photodiode Array
Insights into Sintering with Real Time Correlation of Microstructure Evolution at High-resolution Using X-ray Nano Tomography
Investigation of Microstructure Formation in Plasma Arc Additive Manufacturing Processes by SEM-Based Heating Studies
Key Hole Mode Hunting: Operando Tomographic Microscopy during Laser-based Powder Bed Fusion of Alumina
Leveraging In Situ Synchrotron Radiation Based Imaging to Understand the Impact of Laser Defocusing on Laser Powder Bed Fusion
Machine Learning-driven In Situ Detection of Laser Powder Bed Fusion through Synchrotron and Lab-scale Techniques
Mapping Solidification Pathways in Fe-Ni-Cr Alloys for Additive Manufacturing with Time-Resolved Synchrotron X-ray Diffraction
Microstructural Evolution in Metallic Alloys under Additive Manufacturing Conditions
Neutron Diffraction Analysis of Microstructure and Residual Stresses in Lubricant-free AFSD AA7075 Repairs
Neutron Diffraction Characterization of Additively Manufactured Metals
Neutron Diffraction Microstructural and Deformation Analysis of Additively Manufactured Alloys
New Insights into Laser Additive Manufacturing from Correlative Synchrotron X-ray Imaging at the European Synchrotron
Novel Photometrics Toolbox to Quantify Performance of Versatile X-ray Microscopes
OpeN-AM: A Wire-Arc Deposition System for Operando Neutron Diffraction
Operando Characterization of Laser Powder Bed Fusion of Ti-6Al-4V and Ti-6Al-4V-3Fe via Synchrotron High-speed XRD
Operando X-ray Diffraction Study on Phase Transformations in Carbon Steel during Powder Bed Fusion - Laser Beam
Operando X-ray Imaging of LPBF at X-ray Free Electron Lasers
Probing the Origin of Superelasticity in Metastable Beta Ti-Alloy Using In-situ Synchrotron Diffraction
Refinement Mechanisms of Tantalum-inoculated Aluminum Subjected to Simulated Laser Powder Bed Fusion
Reveal Pore Dynamics during Additive Manufacturing of Oxidized Powders Using Synchrotron X-ray Imaging
Shining Light on LPBF: Schlieren and X-ray Imaging for Melt Pool Dynamics and Process Optimisation
Spatially Resolved Real-time Crystallization Kinetics during Extrusion-based 3D Printing of Semicrystalline Polymers
Spatially Resolving Micro-/Nano- Structures in Bulk Additively Manufactured Parts by Neutron Grating Interferometry
Strain Measurement Using Non-rigid Registration For Mechanical Applications: A Case Study On WAAM-ed Product
The New Capabilities of the Enhanced 32-ID at the APS-U: Opportunities for Additive Manufacturing Research
Time-Resolved Investigation of Martensite Decomposition in Ti-6Al-4V Using In-Situ Synchrotron X-Ray Diffraction
Ultrafine Ti-Fe-based Eutectics for Additive Manufacturing: Pytcho, Micro, and Operando X-ray Imaging for Characterization
Uncovering the Effects of Nanoparticles on the Solidification Dynamics during Laser Melting of Metal by In-situ x-ray Diffraction
Unraveling Microstructural Impacts Governing the Pitting Corrosion Behavior in L-PBF 316L Stainless Steel
Using High-speed Imaging to Inform Process-control Models in Laser Powder Bed Fusion
X-ray Diffraction-computed Tomography (XRD-CT) Facility at NSLS-II for Studying Materials for Nuclear Applications
X-ray Synchrotron Diffraction of 14 Novel Ti-6Al-4V Microstructures Obtained From Post-Build Heat Treatments

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