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Meeting 2024 TMS Annual Meeting & Exhibition
Symposium Nano and Micro Additive Manufacturing
Presentation Title In-situ Studies of Surface Oxide Layer Fracture Upon Powder Particles Flattening
Author(s) Qi Tang, Yuji Ichikawab, Mostafa Hassani
On-Site Speaker (Planned) Qi Tang
Abstract Scope Metallic powder particles are often covered with a native oxide layer on their surfaces. Understanding the fracture behavior of the oxide and its influence on particle mechanical behavior is crucial in a number of processes from powder consolidation to cold spray additive manufacturing. However, the small length-scales involved, i.e., ~10 µm for powder particles and ~10 nm for oxide layers make direct observations challenging. Using a barrel-sputtering technique, we fabricated metallic particles with ~30nm-thick oxide coating. We study particle flattening with in-situ deformation of individual powder particles inside a scanning electron microscope. We resolve the process of oxide layer fracture in-situ and discuss a number of cracking modalities involved. We also complement our real-time observations with finite element simulations to develop a physical understanding of the fracture behavior and the strengthening effects of surface oxide layers.
Proceedings Inclusion? Planned:
Keywords Additive Manufacturing, Powder Materials, Mechanical Properties

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

3D Microarchitectures of Metals, Ceramics, and Polymers, via Droplet-based Nanoprinting for Next Generation Biomedical Devices, Li-ion Batteries, and Robotic Skins
Additive Manufacturing at the Nanoscale - What Are the Materials Challenges?
Aerosol Jet 3D Printed Multi-layered Stretchable Decals for Biomonitoring Applications
Chemical Focusing of Electrochemical Additive Manufacturing: From Micro and Towards Nanoscale
Digitisation of Metal AM for Part Microstructure and Property Control
Direct Out-of-plane Writing of Metals on Insulators by Electron-beam-enabled Electrodeposition with Submicrometer Feature Size
Dynamically Size Droplet Printing (DynaSD): Towards Low-cost, High Value Metal Additive Manufacturing
F-63: Composition Control of Alloy Fabrication Using Localized Electrochemical Deposition for Small-Scale Additive Manufacturing
F-64: Powder Flow Analysis of Copper Nanoporous Micron-sized Powders and Nanoparticles for 3D Printing of Hierarchical Electrodes
Gold Micropillars by Aerosol Jet 3D Nanoprinting Method and Their Behavior Under Compressive Loads
Hydrogel-based Additive Manufacturing of Ceramics and Metals: Simple Chemistries for Advanced Materials
In-situ Resource Utilization of Lunar Highlands Regolith with Graphene Nanoplatelets via Additive Manufacturing
In-situ Studies of Surface Oxide Layer Fracture Upon Powder Particles Flattening
Investigating Governing Size Effect Mechanisms in Ti-6Al-4V Manufactured by Laser Powder Bed Fusion and Electron-Beam Melting
Liquid Metal Dealloying of Additively Manufactured Materials
Manufacturing Size Effect on the Microstructural, Static Mechanical, and Fatigue Properties of Additively Manufactured Ti-6Al-4V Microbeams
Micro Additive Manufacturing of Nd: YAG Ceramic with Optical-gain Properties
Microscale 3D Deposition of Metals by Solid-state Kinetic Bonding
Microstructure Control of Additively Manufacturing Metal Alloys through Microscale Laser Beam Engineering
Novel Approaches for Material and Alloy Design for Metal Additive Manufacturing
Rapid and High-resolution 3D Printing of Solid or Porous Copper Parts with Tunable Nano-porosity Enabled by μCLIP and Nanoporous Copper Powders
Reducing the Scale in Wire and Arc Additive Manufacturing
Size-Effects on Microstructure and Mechanical Properties in LPBF-Fabricated, Thin-walled Hastelloy X and SS316L Components
Strengthening Effect in 3D Architected Ni-Al2O3 Nanocomposite

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