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Meeting 2024 TMS Annual Meeting & Exhibition
Symposium Solidification in External Fields
Presentation Title Structure and Properties of the Terrestrial vs. Microgravity Solders Under Extreme Conditions of Elevated and Cryo Temperatures
Author(s) Manish Kumar, Ralph Napolitano, Sid Pathak
On-Site Speaker (Planned) Manish Kumar
Abstract Scope We report results from the microstructural characterization and resultant micro-to-nano mechanical response of solders under extremes of 1) Earth’s gravity vs. microgravity (1g vs. ~1×10-5g), and 2) cryogenic and 3) elevated temperatures mimicking those experienced during space exploration missions (– 157ēC to +121ēC outside the International Space Station (ISS). Using 40wt%Pb-60wt%Sn solders from the ‘In-Space Soldering Investigation’ conducted onboard ISS, we demonstrate how temperature-induced density gradient and void-induced Marangoni convection during melting/solidification onboard ISS affect its microstructure and properties. Our microscopy and micro-tomography analysis demonstrates a considerable amount of internal porosity (5X terrestrial solder) and accumulation of voids and Pb-rich dendrites toward the high-temperature region in the microgravity solder. Additionally, under cryogenic conditions we examine the effects of β-to-α phase transformation in Sn below 13ēC and the associated volume and internal stress changes in Sn-based solders, while the effects of accelerated aging effects are probed at elevated temperatures (up-to +120ēC).
Proceedings Inclusion? Planned:
Keywords Joining, Solidification, Characterization

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Analogue Study of Nanoparticles' Deagglomeration in Lightweight Alloys Melt
Dynamic Nucleation Events in Zr-2.5Nb during Microgravity Electromagnetic Levitation Experiments
Dynamics of Individual Bubbles in Acoustic Cavitation-induced Solidification Using High-Speed Imaging and Deep Learning
Industrial Trials of Permanent Magnet Stirring during Billet Continuous Casting
Influence of Static Magnetic Field on the Solidification of Inconel 718 Alloys during Additive Manufacturing
Influence of the Coriolis Force on the Macrosegregation of a Steel Alloy
Insights into Phase Refinement via Low-power Electric Current Processing by Synchrotron-based Imaging
Manipulating Flow during Solidification Using Magnetic Fields
Microstructure Control in Additive Manufacturing Using Magnetic Fields and Strategic Scanning
Multiphysics Modelling of the Solidification Dynamics in Pulse Magnetic Fields and Validation by Synchrotron X-ray Imaging
Operando Studies of Phase Nucleation and Growth Dynamics of Metal Alloys in Solidification Under External Fields by Synchrotron X-ray Imaging and Scattering
Solidification of Gallium Indium in Static and Pulsed Magnetic Fields
Solidification of Glass Forming Metallic Liquids Under Aerodynamic Levitation
Structure and Properties of the Terrestrial vs. Microgravity Solders Under Extreme Conditions of Elevated and Cryo Temperatures
The Effects of External Magnetic Field on Keyhole Behavior in Laser Spot Welding of 316L SS Using In-situ X-ray Imaging

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