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Meeting MS&T22: Materials Science & Technology
Symposium Manufacturing and Processing of Advanced Ceramic Materials
Presentation Title Characterization of Early Stage Sintering in Hydroxyapatite via Thermal Conductivity Measurements
Author(s) Anne Leriche, Benoit Nait-Ali, David Smith
On-Site Speaker (Planned) Anne Leriche
Abstract Scope In the last ten years, ceramic densification techniques have been developed, such as spark plasma sintering or microwave assisted heating, to limit grain growth and promote porosity elimination at lower temperatures. If the benefit of using these techniques on the final microstructure has been well established, their impact on the early stages of sintering has not yet been elucidated. The aim of the present work is to follow neck formation and densification in hydroxyapatite ceramics via thermal conductivity evaluation. An analytical model is proposed to describe the thermal conductivity of the green body / partially sintered ceramic in terms of interparticle contact area, porosity, grain size and the intrinsic grain conductivity. Samples were made using conventional sintering, microwave sintering and spark plasma sintering and characterized by laser flash measurements. Finally, the thermal conductivity evolution of a hydroxyapatite green body during the firing cycle is proposed.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Comprehensive Approach to Ceramic Forming Processes
A Novel Approach to Estimate the Hamaker Constant of Ceramic Systems
A Polyvinyl Pyrrolidone Based Binder for PZT Ceramics
Alumina-based Coatings for Metal-cutting Applications
Ceramic Binder Jetting Additive Manufacturing
Characterization of Early Stage Sintering in Hydroxyapatite via Thermal Conductivity Measurements
Cold and Flash Sintering of Metal-doped LLZO for Solid-State Battery Applications
Cold Sintering of Potassium Sodium Niobate, K0.5Na0.5NbO3
Current Progress in Synthesis and Design of Ternary Phases
Densification and Phase Analysis of Zirconium Carbide Ceramics with Different Carbon Contents
Development of CeO2 Stabilized ZrO2 Inks for DIW
Development of Textured UHTC Borides Using Extremely Low Magnetic Fields
Doping Alumina with Carbon?
Fabrication and Microstructure Representation of Heterogeneous Gradient Complex Materials
Flash Sintering of Ceramics: Towards Homogeneous Components with Improved Mechanical Properties
High Throughput, Ultra-fast Laser Sintering of Alumina Sample Array for Establishing the Machine-learning-based Mapping Between Microstructure and Hardness
Impact of Embossing Geometry on the Replication Accuracy of Microchannels in Tape Cast Ceramics
Investigation of Electrical Properties of BaTiO3-PEEK cComposite Processed by Cold Sintering
Investigation of Lamination Approaches for SiC-filled Thermoplastic Polymer Blends
Multi-Material 3D Printing of Ceramics: Process Overview and Successful Trial Examples
Neutron Scattering Visualizing Defects Generation and Structure Recovery in Ball-milled Spinel Oxide
Open Platform Material Development for Additive UV Polymer Manufacturing
Passive pH Control Using Ceramic Particles
Preparation of BaTiO3 Composites by Cold Sintering Process
Process Capability of Lithography-based Ceramic Manufacturing
Processing of High Entropy Garnet Optical Ceramics
Role of Processing and Microstructure on the Phase Transformation in High Entropy Oxides
Surface Area Reduction Behavior of Various Forming Methods of Alumina
The Correlation of Mullite Formation in Porcelains with the Glass Formation Boundary
The Optimization of Field Assisted Sintering Technology and Processing for Ultrahigh Temperature Ceramics for Extreme Environments
Thermal and Mechanical Properties of Freeze-tape Cast Derived Ceramic-metal Composites
Ultra-fast Densification of UHTC ZrB2
Ultrafast High Temperature Sintering of Ceramic Materials for High Temperature Applications
Ultrafast Sintering with and without Electric Fields and Electrochemically Controlled Microstructural Evolution
Utilizing Cold Sintering in the Design and Integration of New Functional Composite Materials

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