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Meeting MS&T21: Materials Science & Technology
Symposium Additive Manufacturing of High and Ultra-High Temperature Ceramics and Composites: Processing, Characterization and Testing
Presentation Title Pathways to Additively Manufacture Ultra-high Temperature Ceramic Composites
Author(s) James W. Kemp, Zlatomir Apostolov, Brett Gibson Compton, Lisa Rueschhoff
On-Site Speaker (Planned) James W. Kemp
Abstract Scope Ultra-high temperature ceramics (UHTC) and their composites (UHTCMCs) are of interest for use in harsh environments encountered by next-generation aerospace vehicles but are limited by their ability to be processed into complex-shaped components. A solution is through additive manufacturing (AM) via direct ink writing (DIW), which allows for the complex shaping of ceramics and composites with high feature resolution. To create complex ceramic shapes, shear-thinning, visco-elastic tailored inks are developed with both preceramic polymers and aqueous slurries and are extruded layer-by-layer. Each set of preceramic- or aqueous-based inks contained zirconium diboride (ZrB2), an UHTC, and various loadings of silicon carbide (SiC) chopped fibers. This study includes an analysis of the rheology and printability of inks and the effects of printing parameters on final ceramic development. Additionally, a description of ceramic conversion processing parameters is given, focusing on porosity comparison between preceramic and aqueous-based inks.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Additive Manufacturing of Aqueous Based Silicon Nitride Suspensions via Direct Writing
Additive Manufacturing of Corrosion Resistant UHTC Materials for Chloride Salt-to-sCO2 Brayton Cycle Heat Exchangers
Additive Manufacturing of High-performance Advanced Ceramics by the Ceramic On-demand Extrusion (CODE) Process
Additive Manufacturing of Silicon Nitride Using a Slurry Approach
Additive Manufacturing of ZrB2–ZrSi2 Composites Using an Electron Beam Melting (EBM) Process
Additive Manufacturing Of ZrB2-SiC Heat Exchanger Geometries by Ceramic on Demand Extrusion
Additive Slurry Drying as a Novel Method for Realizing Large Ceramic Components Using AM
Advanced Polymer-derived (Ultra)-high-temperature Resistant Ceramics and Ceramic Nanocomposites for Additive Manufacturing
AM of UHTCs at LLNL
Binder Jet Additive Manufacturing of Novel Design, High Temperature, Ceramic Heat Exchangers
Ceramic On-demand Extrusion (CODE) of Functionally Graded ZrB2-Mo
Deposition of UHTC Coatings on Refractory Substrates by Directed Energy Methods
High Temperature Properties of Polymer-derived Ceramic Matrix Composites Fabricated via Additive Manufacturing
Innovative Route for the 3D Printing of Hybrid Silicon Carbide/Carbon Fiber Nanocomposites
Investigation of Oxidation Behavior of ZrB2-SiC Composites under Different Partial Pressures of Oxygen
Molten Chloride Salt Corrosion Testing of Ultra High Temperature Ceramics for High Temperature Heat Exchangers Fabricated by Additive Manufacturing Methods
Pathways to Additively Manufacture Ultra-high Temperature Ceramic Composites
Process Development and Optimization for The Laser Powder Bed Fusion of WC-Ni Cermet Composites
Strategies for Printing Continuous Fibers and Post-processing for Ceramic Matrix Composites (CMCs)

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