ProgramMaster Logo
Conference Tools for MS&T23: Materials Science & Technology
Register as a New User
Submit An Abstract
Propose A Symposium
Presenter/Author Tools
Organizer/Editor Tools
About this Abstract
Meeting MS&T23: Materials Science & Technology
Symposium Manufacturing and Processing of Advanced Ceramic Materials
Presentation Title Reaction Flash Sintering of Ti0.5Zr0.5N and Ti0.5Al0.5N Ternary Metal Nitrides
Author(s) Suprabha Das, Andriy Durygin, Vadym Drozd, Md Shariful Islam Sozal , Jesse Smith, Zhe Cheng
On-Site Speaker (Planned) Suprabha Das
Abstract Scope This study aims to demonstrate reaction flash sintering (RFS) for two powder mixtures - TiN-ZrN (both conducting) and AlN-TiN (TiN conducting but AlN insulating), targeting ternary metal nitrides (TMN) of Ti0.5Zr0.5N and Ti0.5Zr0.5N, respectively. A constant DC electrical field of ~50 V/cm and pressure of ~15 MPa at room temperature triggers RFS without pre-heating, and the entire process finishes in a few minutes. Both ex situ XRD and in situ synchrotron studies are carried out to track the phase evolution during RFS and subsequent cooling. Although both systems have a miscibility gap extending to high temperature, uniform Ti0.5Zr0.5N solution formed in RFS persists upon cooling, while (Ti, Al) N solid solution formed at high temperature goes through a quick phase separation in the cooling process. The final products’ microstructure as well as oxidation resistance and mechanical properties are characterized by TGA/DSC, SEM/EDS, Vickers indentation methods.


A Cold Sintering Study of ZnO and Dopants - With a View Towards Varistor Characteristics
Additive Manufacturing of Transparent Optical Ceramics
Basic Research Opportunities from the Army Research Laboratory
Binder Jet Additive Manufacturing for Advanced Ceramics
Ceramic Powder Processing (“Think Like a Particle?” or Perhaps “Think Like a Defect?”)
Densification of Dual Phase High Entropy Boride-Carbide Ceramics by Pressureless Sintering
Design of a Polymer-Metal-Nanoparticle System for Polymer Infiltration and Pyrolysis to Form Ceramic Composites
Design Paradigm for Fabricating MAB Phases
Effect of Binder Phase on TiB2-TiC Based Cermet Materials on the Microstructure and Mechanical Properties
Embedded Printing in Ceramics
Embedded Wire CVD of Silicon Carbide for Homogeneous Joining and SiC-SiC Composite Fabrication
Exploring New Flux Chemistries to Expand the Cold Sintering Process
From Flash Sintering to Ultrafast Sintering without an Electric Field and Electrochemically Controlled Microstructural Evolution
Limitations on the Sintering of Graded Particle Systems
Machine-Learning-Based, Online Estimation of Ceramic’s Microstructure Upon the Laser Spot Brightness During Laser Sintering
Manipulating Instrument Setup Parameters to Increase the Range for Particle Size Measurement
Manufacturing Feasibility of the Cold Sintering Process for Large-scale Ceramic Dielectrics
Measurement of High Temperature Mechanical Property Data for Modeling Applications
Mechanisms of Delamination within Co-extruded Silicon Carbide
Micromechanical Properties and Microstructures of AC and DC Flash-sintered Alumina
Microstructure and Electrical Conductivity of Sol-gel Synthesized and Spark Plasma Sintered Doped-lanthanum Gallate
Nondestructive Materials Characterization Using Ultrasound: Towards a Deeper Understanding of the Cold Sintering Process
Optimizing Ceramic Surfaces for Dust-tolerant Lunar Exploration
Phase and Nanostructure of Polymer Derived Monolithic SiC at Ultrahigh Temperatures
Processing Ceramic Powders in Non-aqueous Mediums - How Polarity of the Suspension Medium Effects Dispersion
Reaction Flash Sintering of Ti0.5Zr0.5N and Ti0.5Al0.5N Ternary Metal Nitrides
Surface Area Reduction During the Sintering of Alumina
Surface Reactivity and Processing Properties of Metal Oxide Nanoparticles for Ceramics
Tailoring Thermal Insulation Ceramic Architectures from Additive Manufacturing
The Influence of Cr on Microstructural Evolution of Alumina
Trends and Opportunities in Manufacturing and Processing of Advanced Ceramic Materials at the National Science Foundation
In Situ Video Monitoring of Zirconium Active Braze Alloy for Joining Al2O3 to Kovar

Questions about ProgramMaster? Contact