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Meeting MS&T23: Materials Science & Technology
Symposium Advanced Characterization of Materials for Nuclear, Radiation, and Extreme Environments IV
Presentation Title In Situ SEM Nanomechanics at Cryogenic Temperatures
Author(s) Eric D. Hintsala, Kevin M. Schmalbach, Sanjit Bhowmick, Douglas D. Stauffer
On-Site Speaker (Planned) Eric D. Hintsala
Abstract Scope Temperature control from cryogenic to room temperature is important for a variety of applications, including aerospace and cold weather automobile performance. Low temperatures always influence mechanical behavior but can also result in more drastic changes such as phase transformations, ductile-to-brittle transitions, and glass transitions. In situ SEM testing enables visualization that’s directly correlated to mechanical data, which helps with their characterization. Furthermore, individual regions of a materials microstructure can be targeted. A low temperature control system has been developed for the Hysitron PI89 that enables continuous control from cryogenic to room temperatures, with independent control on the tip and sample to enable proper temperature matching in vacuum, as is required for elevated temperature testing. Here, the temperature dependent response of two metallic samples are tested at low temperatures, Nitronic 50 and Tungsten.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Accelerated Assessment of Microstructure-Mechanical Property Relationships in Ni Based Superalloys
Accelerated Creep Testing for High-Temperature and Nuclear Applications
Advanced In-situ Strain Mapping for Zr Oxidation by 4D-STEM
Assessing the Ability of Nuclear Fuel Performance Codes to Predict Radially Resolved Properties in Oxide Fuels
Capturing 3D Evolution of Twin Networks in Titanium as a Function of Applied Strain
Effect of Solutes on the Radiation Induced Segregation in Ferritic Alloys at ∑3- grain Boundaries
Effect of Strain Rate on Tensile Properties of C250 Maraging Steel
Enabling Multiscale Materials Characterization with Machine Learning
Four-dimensional Scanning Transmission Electron Microscopy (4D-STEM) Characterization of Intergranular Corrosion of Austenitic Stainless Steels in Lead-bismuth Eutectic
High-Temperature Irradiation Behavior of Piezoelectric Aluminum Nitride
In Situ SEM Nanomechanics at Cryogenic Temperatures
Interdiffusion Behaviour of UN with Zircaloy-4 via Diffusion Couple Studies
M-1: Novel Method for Fabricating and Analysis of 3D Printed Composite for Radiation Shielding Containing Metalized Halloysite Nanotube
Mapping Elemental Distributions Across Thin Corrosion Films Formed on Nuclear Reactor Core and Structural Materials via Ex-situ And In-situ Atom Probe Tomography
Multimodal Characterization of Materials Corrosion in Molten Salts
Phase Stability of Delta-ZrH Under Ion Irradiation
Probing Nanoscale Properties of Radioactive Material by Advanced Correlative Microscopy
STEM-based Mapping of Nanoscale Point Defects Produced via Temperature, Irradiation, And Corrosion
Structural Stability of REE-PO4 (REE=Sm,Tb) under Swift Heavy Ion Irradiation
Thermodynamic Modeling and Calculation of Phase Formation Processes Under Irradiation Conditions of Uranium-plutonium Nitride Fuel
Transition Metal Carbonitride Materials Exposed to Swift Heavy Ions

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