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Meeting MS&T23: Materials Science & Technology
Symposium Advanced Characterization of Materials for Nuclear, Radiation, and Extreme Environments IV
Presentation Title Accelerated Assessment of Microstructure-Mechanical Property Relationships in Ni Based Superalloys
Author(s) Kevin Schmalbach, Toshio Osada, Eric Hintsala, Douglas Stauffer, Takahito Ohmura
On-Site Speaker (Planned) Kevin Schmalbach
Abstract Scope Understanding the mechanical properties of individual phases of multi-phase materials can often be hindered by the process of aligning separately measured microstructure and mechanical property maps, especially for high temperature applications. Here we discuss the development and utilization of a novel system designed to streamline the identification of microstructure-mechanical property relationships. The system is a Hysitron PI89 Picoindenter system using a rotation and tilt stage to navigate between EBSD for microstructure identification and nanoindentation positions to assess site-specific material properties. This can be coupled with a heating stage capable of attaining 1000 °C to directly assess the relationships between temperature, phase/orientation, and mechanical properties. Finally, we will apply the new system to understand phase transformations and temperature dependence of mechanical properties at elevated temperatures in nickel based superalloys.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Accelerated Assessment of Microstructure-Mechanical Property Relationships in Ni Based Superalloys
Accelerated Creep Testing for High-Temperature and Nuclear Applications
Advanced In-situ Strain Mapping for Zr Oxidation by 4D-STEM
Assessing the Ability of Nuclear Fuel Performance Codes to Predict Radially Resolved Properties in Oxide Fuels
Capturing 3D Evolution of Twin Networks in Titanium as a Function of Applied Strain
Effect of Solutes on the Radiation Induced Segregation in Ferritic Alloys at ∑3- grain Boundaries
Effect of Strain Rate on Tensile Properties of C250 Maraging Steel
Enabling Multiscale Materials Characterization with Machine Learning
Four-dimensional Scanning Transmission Electron Microscopy (4D-STEM) Characterization of Intergranular Corrosion of Austenitic Stainless Steels in Lead-bismuth Eutectic
High-Temperature Irradiation Behavior of Piezoelectric Aluminum Nitride
In Situ SEM Nanomechanics at Cryogenic Temperatures
Interdiffusion Behaviour of UN with Zircaloy-4 via Diffusion Couple Studies
M-1: Novel Method for Fabricating and Analysis of 3D Printed Composite for Radiation Shielding Containing Metalized Halloysite Nanotube
Mapping Elemental Distributions Across Thin Corrosion Films Formed on Nuclear Reactor Core and Structural Materials via Ex-situ And In-situ Atom Probe Tomography
Multimodal Characterization of Materials Corrosion in Molten Salts
Phase Stability of Delta-ZrH Under Ion Irradiation
Probing Nanoscale Properties of Radioactive Material by Advanced Correlative Microscopy
STEM-based Mapping of Nanoscale Point Defects Produced via Temperature, Irradiation, And Corrosion
Structural Stability of REE-PO4 (REE=Sm,Tb) under Swift Heavy Ion Irradiation
Thermodynamic Modeling and Calculation of Phase Formation Processes Under Irradiation Conditions of Uranium-plutonium Nitride Fuel
Transition Metal Carbonitride Materials Exposed to Swift Heavy Ions

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