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Meeting MS&T21: Materials Science & Technology
Symposium Manufacturing and Processing of Advanced Ceramic Materials
Presentation Title A Novel Room-temperature Synthesis Technique for Producing High-density Electroceramic Composites
Author(s) Evan C. Smith, Rick Ubic
On-Site Speaker (Planned) Evan C. Smith
Abstract Scope Room-temperature fabrication represents a major technological leap in ceramic processing techniques. This procedure has the potential to save a significant amount of energy because it avoids use of the high temperatures needed for conventional ceramic sintering techniques. In this work, a novel approach is taken to achieve high densities (>90%) in ceramic compacts at room temperature. The electroceramic filler material (Ba<sub>x</sub>Sr<sub>1-x</sub>TiO<sub>3</sub> or PbZr<sub>1-y</sub>Ti<sub>y</sub>O<sub>3</sub>) is mixed with an aqueous solution of a dielectric binder material (<i>e.g.</i> Li<sub>2</sub>MoO<sub>4</sub>) and pressed in a cylindrical die under high pressure and high vacuum using a vacuum-assisted uniaxial press. The die is then immersed in a bath sonicator for various times, after which it is pressed again. A major advantage of this technique is that it uses a relatively small amount of binder material (~15vol%); thus, the electroceramic filler material is the dominant phase in the resultant composite pellets.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Novel Room-temperature Synthesis Technique for Producing High-density Electroceramic Composites
Analysis of Crystal Structure in Calcium and Strontium Hexaborides with Lithium Dopants
Aqueous Colloidal Processing of WC Based Materials with Alternative Metals as Sintering Aids or Binder
Bulk Amorphous SiCN Produced through Plasma Synthesis and Spark Plasma Sintering
Chemical Vapor Deposition of Zirconium-silicon-carbon Compositions
Comparison of Microstructural Evolution of Hydroxyapatite Powder Sintered by Microwave, SPS and Conventional Sintering
Development Calcium Doped La(Cr0.2Co0.2Fe0.2Mn0.2Ni0.2)O3 High Entropy Perovskite Oxides
Development of New Synthesis Route for Environmentally Friendly Thermoelectric Rare Earth Borocarbonitrides for Upcoming Carbon-neutral Society
Dispersion Studies of Alumina Toughened Zirconia Powders for Direct Ink Writing Applications
Effects of Sintering Additive and Oxygen Partial Pressure on Solid-state Single-crystal Growth of YAG Ceramics
Flash Sintering, Ultrafast Sintering without Electric Fields, and Electric Field Effects on Microstructural Evolution
Green State Joining of Silicon Carbide for High-temperature Applications
High Temperature Coatings for Concentrated Solar Power Receivers
Issues Related to the Manufacturing and Processing of Refractory Ceramic Materials
Leveraging Computational Thermodynamics for Guiding SiC-ZrC Chemical Vapor Deposition Process Development
Low Energy Syntheses of Ceramic Powders and Composites
Low Temperature Synthesis Methods for Nanoparticle Carbides
Luminescence Thermometry - Striving a Breakthrough
Making Pre-stressed Ceramics with High Strength and High Damage Tolerance
Mechanical Properties of La2Zr2O7/ ZrO2 Composites Prepared by Coating of ZrO2 Sol
Pressureless Sintered SiC Formed via Thermoplastic Fugitive Binders for High-temperature Applications
Progress of Silicon Nitride: Processing, Structure and Property
Recent Progress in Fusion Welding of Structural Ceramics and Composites
Selective Laser Sintering of Hexagonal Barium Titanate Ceramics
Self-propagating High Temperature Synthesis of Chevrel Phase Compounds
Spark Plasma Joining of HfB2-ZrB2-SiC Composites Using Ni as a Filler
Surface Stengthening of Single-crystal Alumina by High-temperature Laser Shock Peening
Textured UHTC Borides Using Extremely Low Magnetic Fields
The Future of Manufacturing in Energy-intensive Industries
Ultra-fast Laser Sintering of Alumina and the Microstructure Prediction Based on Machine Learning
Unique Technological Advantages and Progress towards Manufacturing Scale-up

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