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Meeting 2023 TMS Annual Meeting & Exhibition
Symposium High Temperature Electrochemistry V
Presentation Title The Impact of Moisture on the Electrochemical Behavior of Molten Calcium Chloride
Author(s) Marah Fuller, Devin Rappleye
On-Site Speaker (Planned) Devin Rappleye
Abstract Scope The presence of moisture in molten salts impacts their electrochemical and corrosion behavior. However, systematic studies on the effect of moisture on the electrochemical behavior of molten salts using electroanalytical techniques are lacking. This work seeks to provide an analysis of moisture within molten calcium chloride through various electrochemical methods. Cyclic voltammetry, square wave voltammetry, and chronoamperometry are performed and their associated relations are applied to characterize the behavior of hydrogen ions in molten calcium chloride. Also, Karl Fischer titration and electrochemical signals are also investigated as a potential ex-situ and in-situ methods, respectively, to quantify the moisture content of various samples from pure, molten CaCl2 containing differing amounts of moisture.
Proceedings Inclusion? Planned:
Keywords Electrometallurgy, Characterization, Pyrometallurgy

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Revised High Temperature Synthesis of UCl3 via Reaction of U with FeCl2
Blind Identification and Quantification of Analytes in Molten LiCl-KCl Eutectic
Chloro-aluminate Species Distribution Correlation with Electrical Conductivity of 1-ethyl-3-methyl Imidazolium Chloride (EMIC)-Aluminum Chloride (AlCl3) System
Cyclic Voltammetry for Real-time Oxide Ion Concentration Measurements of a Molten CaCl2
Electrochemical Behavior of Bismuth in molten LiCl-KCl-CaCl2
Electrochemical Properties of Ca-Sb Metal Battery with a Molten Chloride Electrolyte
Electrochemical Reduction of Nd2O3+Fe2O3 Mixed Oxide Precursors in Calcium Chloride Melt
Evaluating the Effects of Mixed Cation Molten Salt Electrolytes within the Li-Sb-Sn Liquid Metal Battery System
Evaluating the Electrochemical Recovery of Gd Using a Reactive Liquid Bi Electrode
Formation of Carbon Layer on Ni and Mo Through Electrochemical Reduction of Carbonate Ions in Molten LiCl
Numerical Modelling and Phase Field Modelling of Silicon Electrodeposition for Solar Cells at High Temperatures using Molten Salts
On the Separation of Niobium and Tantalum Metals via Molten Sulfide Electrolysis
Optimisation of the Anodic and Cathodic Current Densities during Nd Electrowinning Process
Oxide Ion Ceramic Sensor in Molten CaCl2 for Real Time Monitoring of the Direct Oxide Reduction Process
Relative Performance of Platinum, Iridium, and Ruthenium as Oxygen-Evolving Anodes during the Electrolytic Reduction of Uranium Oxide in Molten LiCl-Li2O
Study of Potentiometry for Monitoring Activity of GdCl3 in Molten LiCl-KCl Salt
The Demonstration and Optimization of Thin-cell Electrochemical Measurements in Molten LiCl-KCl Eutectic
The Impact of Moisture on the Electrochemical Behavior of Molten Calcium Chloride
Thermodynamic Properties of Nd-Fe Alloys via EMF Measurements in Molten Salts

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