About this Abstract |
Meeting |
2023 TMS Annual Meeting & Exhibition
|
Symposium
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Characterization of Minerals, Metals and Materials
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Presentation Title |
Fabrication and Structural Analysis of BaTiO3 Based Solid Solutions Codoped with La3+ and Bi 3+ |
Author(s) |
María Inés Valenzuela Carrillo, Miguel Pérez Labra, Ricardo Martínez López, José Antonio Romero Serrano, Francisco Raúl Barrientos Hernández, Martin Reyes Pérez, Julio Cesar Juárez Tapia, Aurelio Hernández Ramírez, Gustavo Urbano Reyes |
On-Site Speaker (Planned) |
María Inés Valenzuela Carrillo |
Abstract Scope |
The structural evolution of solid solutions BaTiO3-type doped with La3+ and Bi 3+ was investigated. The samples were prepared according to the formula Ba1-3xLa2xTi1-3xBi4xO3 for the compositions x = 0.0, 0.001, 0.0015, and 0.002 of La3+ and Bi 3+ (wt. %) and were synthesized by the ball milling method. Then, the powder mixture was sintered with a thermal ramp of 4°C/min for 5 hours and maintained at 1200°C for 5 more hours. The structural properties of synthesized doped BaTiO3 were characterized by means of X-ray diffraction (XRD) and scanning electron microscopy (SEM). The analysis of XRD patterns revealed the presence of tetragonal BaTiO3(96-150-7757) and allowed to calculate the lattice parameters (a, c) for each composition. The volume of the unit cell decreased for the x>0.0 compositions in comparison to pure BaTiO3 which can be attributed to the addition of the ions La3+ and Bi 3+ in the BaTiO3 structure. |
Proceedings Inclusion? |
Planned: |
Keywords |
Characterization, Ceramics, Powder Materials |