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Meeting 2020 TMS Annual Meeting & Exhibition
Symposium Advanced Real Time Imaging
Presentation Title In-situ Heating S/TEM Observations of Weld Microstructure Evolution in Ni-30Cr Alloy with Tantalum and Molybdenum Additions
Author(s) Cheng-Han Li, Sriram Vijayan, Carolin Fink, Joerg R Jinschek
On-Site Speaker (Planned) Cheng-Han Li
Abstract Scope Microstructural evolution in Ni-30Cr weld metal with Ta and Mo additions upon in-situ heating was investigated using scanning/transmission electron microscopy (S/TEM). Ni-30Cr filler metals are commonly used for repair of structural components in nuclear power industry, but are somewhat prone to weld cracking, in particular in multi-pass repair applications. Intergranular cracking is effected by precipitation of secondary constituents along grain boundaries upon reheating of deposited weld metal. In-situ heating experiments in the TEM were performed to study the precipitation and transformation behavior under conditions that mimic thermal cycling during multi-pass welding. A MEMS-based heating holder was used to allow for controlled heating and cooling experiments with high spatial resolution. The significance of these in-situ observations for selection of filler metal composition and weld process parameters that yield desirable microstructures are discussed.
Proceedings Inclusion? Planned:

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