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Meeting 2020 TMS Annual Meeting & Exhibition
Symposium Use of Large Scale Facilities to Understand the Physical Metallurgy of Fe-based Alloys
Presentation Title HEXRD and SAXS to Unveil the Dynamics of Phase Transformation in Steels: From Carbide-free Bainite To Mapping of Compositionally Graded Samples
Author(s) Imad-Eddine Benrabah, Z. Tournoud, Frédéric Bonnet, Frederic De Geuser, Alexis Deschamps, D. Huin, P. Donnadieu, Hugo Van Landeghem
On-Site Speaker (Planned) Alexis Deschamps
Abstract Scope This presentation will illustrate how the use of synchrotron in-situ experiments helps to reach a quantitative characterization of phase transformations in steels. First, in-situ high energy X-ray diffraction (HEXRD) and in-situ small-angle X-ray scattering (SAXS) will be applied to follow how the bainite transformation in TRIP-aided bainitic steels is modified by the addition of microalloying (V or Nb). HEXRD is used to follow the austenite and ferrite phase fractions as well as the carbon content of austenite. SAXS is used to follow the formation of nanometer-scale transition carbides. In the second part of this talk, we will show that the in-situ HEXRD experiments can be extended to be spatially-resolved on compositionally-graded steels, in order to achieve by a combinatorial approach a map of phase transformation kinetics in compositional space. Fe-X1-X2-C alloys with composition gradients have been obtained, where Xi=(Mn, Mo, Cr, Si). The evolution of austenite and ferrite phase fractions have been followed in these gradients in-situ during inter-critical annealing, in order to evaluate the solute drag effect when several substitutional species are involved.
Proceedings Inclusion? Planned: Supplemental Proceedings volume

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Carbide-free Bainite Transformations in Non-isothermal Conditions Investigated by In-situ High-energy X-ray Diffraction Experiments
Carbon Heterogeneities in Austenite during Quenching & Partitioning (Q&P) Process Revealed by In Situ High Energy X-ray Diffraction (HEXRD) Experiments
HEXRD and SAXS to Unveil the Dynamics of Phase Transformation in Steels: From Carbide-free Bainite To Mapping of Compositionally Graded Samples
In-situ Synchrotron X-ray Diffraction Stress Analysis during Laser Surface Line Hardening of Samples with Specific Geometric Features
In situ HEXRD Determination and Numerical Simulation of Internal Stresses during HeatTtreatment of Carburized and Carbonitrided Low-alloyed Steels
In situ Quantitative Study of Retained Austenite Mechanical Stability in 3rd Generation TRIP-aided Steels by High-Energy X-ray Diffraction on Synchrotron Beamline
Microstructure Evolution and Phase Transformations during Deformation of Metastable Austenitic CrMnNi Steel as Revealed by In situ Synchrotron Radiation X-ray Diffraction
Nucleation and Evolution of Sigma Phase and Nitrides during Heat Treatment and Welding of Duplex Stainless Steels
Precipitation Kinetics and Chemistry Evolution of Oxide Dispersion Strengthened Steels throughout their Consolidation Process Evaluated by In-situ Anomalous Small-angle X-ray Scattering
Real-time Investigation of Recovery, Recrystallization and Austenite Transformation during Annealing of a Cold-rolled Steel Using High Energy X-ray Diffraction (HEXRD)
Stress Tensor Determination during Phase Transformation of a Metal Matrix Composite using In situ High Energy X-ray Diffraction

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