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Meeting 2020 TMS Annual Meeting & Exhibition
Symposium Use of Large Scale Facilities to Understand the Physical Metallurgy of Fe-based Alloys
Presentation Title In-situ Synchrotron X-ray Diffraction Stress Analysis during Laser Surface Line Hardening of Samples with Specific Geometric Features
Author(s) Dominik Kiefer, Jens Gibmeier, Fabian Wilde, Felix Beckmann
On-Site Speaker (Planned) Jens Gibmeier
Abstract Scope Recently, a synchrotron X-ray diffraction based measuring strategy was established for real time monitoring of local stress development and phase transformations during laser surface hardening of steel samples. Here, we report about AISI 4140 steel samples that were line hardened using a 4 kW high power diode laser while controlling the maximum surface temperature. In-situ X-ray diffraction analyses during temperature controlled laser hardening experiments were carried out at the synchrotron beamline P05@PETRAIII at DESY in Hamburg using a photon energy of 10.9 keV. Local phase transformation kinetics and stress evolution at the sample surface were monitored at a rate of 50 Hz with a spatial resolution of <Ø1 mm. To quantify sample geometry effects on the stress formation and hence the residual stress state in the process zone, samples with specific geometric features (surface curvatures with defined radii and bridged structures) were investigated and compared with results of flat specimen.
Proceedings Inclusion? Planned: Supplemental Proceedings volume

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Carbide-free Bainite Transformations in Non-isothermal Conditions Investigated by In-situ High-energy X-ray Diffraction Experiments
Carbon Heterogeneities in Austenite during Quenching & Partitioning (Q&P) Process Revealed by In Situ High Energy X-ray Diffraction (HEXRD) Experiments
HEXRD and SAXS to Unveil the Dynamics of Phase Transformation in Steels: From Carbide-free Bainite To Mapping of Compositionally Graded Samples
In-situ Synchrotron X-ray Diffraction Stress Analysis during Laser Surface Line Hardening of Samples with Specific Geometric Features
In situ HEXRD Determination and Numerical Simulation of Internal Stresses during HeatTtreatment of Carburized and Carbonitrided Low-alloyed Steels
In situ Quantitative Study of Retained Austenite Mechanical Stability in 3rd Generation TRIP-aided Steels by High-Energy X-ray Diffraction on Synchrotron Beamline
Microstructure Evolution and Phase Transformations during Deformation of Metastable Austenitic CrMnNi Steel as Revealed by In situ Synchrotron Radiation X-ray Diffraction
Nucleation and Evolution of Sigma Phase and Nitrides during Heat Treatment and Welding of Duplex Stainless Steels
Precipitation Kinetics and Chemistry Evolution of Oxide Dispersion Strengthened Steels throughout their Consolidation Process Evaluated by In-situ Anomalous Small-angle X-ray Scattering
Real-time Investigation of Recovery, Recrystallization and Austenite Transformation during Annealing of a Cold-rolled Steel Using High Energy X-ray Diffraction (HEXRD)
Stress Tensor Determination during Phase Transformation of a Metal Matrix Composite using In situ High Energy X-ray Diffraction

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