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Meeting 2021 TMS Annual Meeting & Exhibition
Symposium Advanced Real Time Imaging
Presentation Title Direct Observation of Boron Nitride Dissolution in a Heat Resistant Martensitic Steel Using Confocal Scanning Laser Microscopy
Author(s) Andrew (Drew) Huck, Bryan Webler
On-Site Speaker (Planned) Andrew (Drew) Huck
Abstract Scope Boron and nitrogen have become increasingly important in modern steels to impart greater creep resistance in forged products for elevated temperature applications. During solid-state processing, these two elements can combine under certain conditions and form coarse boron nitrides (BN), which can negatively impact properties and decrease the effect of these elements on creep resistance. Dissolution of these features in a heat-resistant martensitic steel has been observed in controlled furnace heat treatments. This study attempts to observe real time dissolution of BN particles using confocal scanning laser microscopy (CSLM) to confirm the thermodynamic stability range of these particles, which has been modeled using ThermoCalc. CSLM is a technique that allows surface observation with controlled temperature and atmospheric conditions, which should allow direct optical observation of these features. This should inform future heat treatment practices and expand knowledge of the thermodynamics of these particles.
Proceedings Inclusion? Planned:
Keywords Iron and Steel, Phase Transformations, High-Temperature Materials

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Characterizing Laser-driven Metal Ejecta Interactions
Determination of Uranium Oxidation Kinetics Through White-Light Interferometry
Direct Observation of Boron Nitride Dissolution in a Heat Resistant Martensitic Steel Using Confocal Scanning Laser Microscopy
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In-situ Real Time Observation of Austenite Formation in Duplex Stainless Steels during Different Cooling Conditions
In Situ Characterization of the Balling Phenomenon in Additive Manufacturing
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