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Meeting 2023 TMS Annual Meeting & Exhibition
Symposium 2023 Technical Division Student Poster Contest
Presentation Title SPG-37: Oxide Morphology and Growth Kinetics for Additively Manufactured 316L Austenitic Stainless Steel High Temperature Steam Exposures
Author(s) Scott Schier, Katherine Montoya, Allyssa Bateman, Ethan Schneider, Elizabeth Sooby, Brian Jaques
On-Site Speaker (Planned) Scott Schier
Abstract Scope Additive manufacturing (AM) has been proposed as a multifaceted approach to high throughput and material characterization and testing to relate print parameter, print orientation, sample, and thermal histories to relevant nuclear reactor performance properties. Continuous research in AM has propelled it to revolutionize the manufacturing industry due to the unparalleled design flexibility of the build process that allows rapid innovation of complex parts. Reactor parts are required to meet structural material qualifications meaning AM parts must be able to withstand off-normal reactor events involving steam exposure, in light water reactors as well as some advanced reactor designs. This study presents the characterization of oxidized AM 316LSS when exposed to high temperature (600C<T<1000C) steam (<65% pH2O) atmospheres. Raman spectroscopic analysis determines the chemical composition of the polished/passivated surface oxides that form on samples. Scanning electron microscopy provides microstructural characterization of surface and cross-sectional features of the oxide films and pitting defects.
Proceedings Inclusion? Undecided
Keywords Additive Manufacturing, High-Temperature Materials, Characterization

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

SPG-11: Optimized Design of Interlocking Metasurfaces
SPG-12: Synthesis and Characterization of Fullerene-Antibody Conjugate Energetic Nanoparticles (FACE-NP) for Bladder Cancer Treatment
SPG-15: Transition Mechanism for the Metastable Phases in Al-Zn-Mg Alloys: A Novel Molecular Dynamics Approach
SPG-16: A Computer Vision Method of Grain Segmentation for Additive-manufactured Haynes 282 Alloys Under Various Heat Treatments
SPG-17: Characterization of Failure Mechanisms for Multimaterial Interfaces Manufactured with Additive Friction Stir Deposition
SPG-18: Characterization of Microstructural Heterogeneities in Electron Beam Additively Manufactured Haynes 282
SPG-19: Comparison of Experimental and Analytical Melt Pool Geometries for High Thermal Conductivity Refractory Metals Using ANSYS
SPG-1: Determination of Mechanical, Thermal and Barocaloric Properties of Elastomers by Rheological Techniques for Hydrostatic Pressure based Solid State Refrigeration
SPG-20: Correlating Laser Process Conditions to Balling Severity with Time-Resolved Synchrotron X-ray Visualization
SPG-21: Development of a Generalized Fatigue Assessment Approach for Steel Castings
SPG-22: Effect of Chemical Pretreatment on Properties of Natural Fiber Reinforced Composites for 3D Printing
SPG-23: Effect of Laser Surface Remelting on the Microstructure, Mechanical, Tribological and Corrosion Properties of Bio-applicable Ti40Nb25Zr25Ta10 Medium Entropy Alloy (MEA) with 0.5 at. % O
SPG-24: Effect of Process Parameters on Texture and Anisotropy of Ti-6Al-4V Wall Components Made by Wire-feed DED Process
SPG-25: Effects of the Reduction Temperature and Amount of Diluent on the Properties of High-purity Tantalum Powder Prepared via the Hunter Process
SPG-26: Effects of Varying Heat Accumulation in Laser Powder Bed Fusion on Microstructure Outcomes in Ti-6Al-4V
SPG-27: Evaluating the Effect of Tool Offset on Repaired AA7050 by Additive Friction Stir Deposition
SPG-28: Evaluation of As-deposited Tensile Behavior and Microstructure of Additive Friction Stir Deposition 304L Stainless Steel
SPG-29: In Operando Synchrotron X-ray Tomography Study of Fine Eutectic Polyphase Solidification Patterns
SPG-2: Extraction of Niobium and Tantalum Oxides from Columbite Concentrate
SPG-30: Induction-Coupled Thermomagnetic Processing of Fe-C Alloys
SPG-31 Laser-Powder Bed Fusion of Ti-6Al-2Sn-4Zr-2Mo-0.08Si (Ti-6242): As-built Properties, Kinetics of α to β Phase Transformation, and Design of Heat Treatment
SPG-32: Melt-pool Dynamics during Multiple-laser-beamed Powder Bed Fusion of Stainless Steel
SPG-33: Modeling for Time Dependent Grain Boundary Evolution
SPG-34: Multi-scale In Situ Studies of Deformation Mechanism of L-PBF 316L Stainless Steels
SPG-36: On the Influence of Gaussian and Ring-shaped Beam Profiles on Quality and Energy Consumption in L-PBF of Inconel 718
SPG-37: Oxide Morphology and Growth Kinetics for Additively Manufactured 316L Austenitic Stainless Steel High Temperature Steam Exposures
SPG-38: Printability and Defects in W & W -alloys by Directed Energy Deposition
SPG-39: Recycled Battlefield Titanium Scrap for Cold Spray Applications
SPG-3: Flexural Properties of Low Density Polyethylene Hybrid Nanocomposite Reinforced with Linen and Aramid Fabric
SPG-40: Removal of Rare Metal Impurities by Electron-beam Melting Refining Process
SPG-41: Strain Evolution and Damage Development during Tight-radius Bending of Advanced High Strength Steels
SPG-44: Advanced Characterization of the Local Atomic Orders and Their Effects on the Mechanical Properties in Metallic Glasses
SPG-45: Atomistic Modeling of Energy Barriers to Dislocation Processes in Metals
SPG-46: Automating Selective Area Electron Diffraction Pattern Phase Identification Using Image Analysis and Machine Learning
SPG-47: Bulk Material Libraries through Laser-Remelting: Combinatorial Analysis of the CrCoNi System
SPG-48: Corrosion Control of Structural Materials for 4th Gen Nuclear Reactors
SPG-49: Deformation Mechanism Characterization for Bi-modally Distributed γ' Precipitates in Allvac 718plus Superalloy
SPG-4: Phytomining of Rare Earth Elements
SPG-50: Effect of Ag on the Microstructures in Al-Cu-Ni-Mn High Entropy Alloy
SPG-51: Experimental Observation of Heteroepitaxial Recrystallization (HeRX) outside of Low Lattice Misfit Ni-based Superalloys
SPG-52: Investigation of Corrosion Mechanisms and Fatigue Property of Friction-stir Welded Joints between 6022 Al and ZEK100 Mg Alloy
SPG-54: Microstructural Characterization and Oxidation of Non-BCC High Entropy Alloys
SPG-55: Modeling of Non-equilibrium Phenomena in Laser Additive Manufacturing Using Molecular Dynamics
SPG-56: Nanoscale Differences in Tooth Enamel with Aging by Atom Probe Tomography
SPG-57: Sintering and Densification Mechanism of HfB2 Based Ultra High Temperature Ceramics for Hypersonic Space Vehicles
SPG-58: Thermal Stability of Novel Multicomponent Al-based High-performance Alloys and Its Direct Implication on Their Mechanical Properties
SPG-59: Understanding Nanostructures in the Binary Ti-Fe Alloy Using Advanced Electron Microscopy
SPG-5: Selective Recovery of Copper from Metal Concentrate of Waste Printed Circuit Boards by Ammoniacal Solvo-leaching
SPG-60: Understanding the Microstructural Evolution in the Modeled Ti-18Mo-5Al Alloy Using Scanning Electron Microscopy
SPG-6: Electronic Transport Properties of Mn2Sb
SPG-7: First-Principles Study of Vacancy Formation Energy in High-Entropy Alloys
SPG-8: Investigation of Functional Coatings for Improving Performance of Carbon Nanotube-based Supercapacitors
SPG-9: Material-based Characterization of Carbon Nanotube Field Emission Cathodes
SPU-10: Mechanochemistry for Creation of Functional Surface Treatments
SPU-11: Study of the Pyrometallurgical Recycling Process to the Recovery of Zinc and Manganese Oxide from Spent Alkaline and Zn-C Batteries
SPU-12: Viscosity Characterization of an Energetic Initiator Ink for 3D Printing
SPU-13: An In-situ Radiography Study on Meltpool Dynamics and Fluid Flow as a Function of Laser Power in Ti-6Al-4V Raster Melts
SPU-14: Understanding the Microstructure-Property Relationship in the Additive Manufactured Titanium Alloy for Aerospace Applications
SPU-15: Using Microstructural Modifications to Influence Intense Strain Localization in Inconel 718Plus
SPU-1: Cultural Heritage Science: Authentication of Native American Artwork via Materials Characterization and Forensic Analysis
SPU-2: Investigation of High Entropy Precursor Powder Synthesis for Transparent Ceramic Synthesis
SPU-3: Correlating Local and Global Tensile Deformation Behavior of AlSi10Mg Specimens Fabricated Via Laser Powder Bed Fusion
SPU-4: Developing a Metallography Procedure to Investigate Compositional Effects on the Microstructure of Lightweight Metal Matrix Composites
SPU-5: A High-speed Radiography Study for Validating the Effect of Dwell Time on Melt-pool Dynamics during Laser Powder Bed Fusion
SPU-6: Assessing Laser Powder Bed Additive Manufacturing Part Quality via In-Situ Monitoring & Machine Learning
SPU-7: Burn Rate Analysis of an Energetic Initiator Ink for 3D Printing
SPU-8: Development of a Pyrotechnic Initiator Ink for Additive Manufacturing Methodology
SPU-9: Effects of LPBF Parameters on Fatigue Life of AlSi10Mg Alloys

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