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Meeting 2020 TMS Annual Meeting & Exhibition
Symposium Mechanical Response of Materials Investigated through Novel In-situ Experiments and Modeling
Presentation Title Synthesis and Mechanical Behavior of Freestanding NiTi Films with Varying Grain Sizes
Author(s) Paul Rasmussen, Jagannathan Rajagopalan
On-Site Speaker (Planned) Paul Rasmussen
Abstract Scope Here, we describe a new process to synthesize thin films with precise microstructural control via systematic, in-situ seeding of nanocrystals, and subsequent crystallization of amorphous precursor films. Based on this process, we synthesized Cr-seeded NiTi films with nanocrystalline and submicron grain sizes, and different phase compositions by methodically varying the annealing treatments. We then co-fabricated freestanding samples of the films with MEMS testing stages and performed cyclic tensile load-unload experiments. While all samples exhibited the shape-memory effect, the underlying deformation mechanisms were notably different. Films with submicron grains that initially had a mixed austenite/martensite microstructure deformed via a combination of phase transformation of austenite grains alongside detwinning of martensite grains. The nanocrystalline films initially had a fully austenitic microstructure and deformed via combination of phase transformation and plasticity. Preliminary in-situ TEM straining suggest that inelastic strain recovery in these films is caused by both reverse phase transformation and reverse plasticity.
Proceedings Inclusion? Planned: Supplemental Proceedings volume

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A Novel Fracture Observation in SiC-based Ceramics Through In-situ Double Torsion Testing
A Novel X-ray Diffraction Simulation Framework for Rapid Thermo-mechanical Processes
Ab-initio Predictions of Plastic Anisotropy in BCC Metals
Acoustic Emission Measurements During In-situ Scanning Electron Microscopy Experiments to Quantifying Damage Accumulation and Crack Initiation in Microcrystals
Assessing Crack Propagation Along Brittle/Ductile Interfaces
Core Structure and Mobility of Dislocations in Alpha-Ti
Deformation Behavior of Additively Manufactured Cu-Fe Composites at Different Strain Rates
Development of TiAl Alloys for High Temperature Applications
Dislocation-grain Boundary Interaction Investigations Using In-situ DIC and EBSD
Effect of Loading Rate on Fracture Behavior of Magnesium Alloys
Examination of Local Microscale-microsecond Temperature Rise in HMX-HTPB Energetic Material under Impact Loading
Experimental and Numerical Investigation into Mechanical Degradation of Polymers and Polymer Composites
Fabrication of Microscale Specimens via Additive Manufacturing for In-situ Mechanical Testing
Fracture Across Length Scales in Tungsten: A Combined Experimental and Predictive Approach
High Throughput Creep Data Acquisition by Cantilever Bending Coupled to Digital Image Correlation
Impact of the Architecture / Texture on the Mechanical Behavior of Ni-microwires: How to Drive the Strength and Ductility
In-situ Dynamic Stress Field Detection using 2D Mechanical Raman Spectroscopy
In-situ Mechano-electrochemical Coupling of Structural Supercapacitor Electrodes
In-situ TEM Investigation of the Electroplasticity Phenomenon in Metals
In-situ TEM Investigation on Pyramidal Dislocations in Magnesium
Investigating Bulk Mechanical Properties on a Micro-scale: Micro-tensile Testing of Ultrafine Grained Ni-SiC Composite to Determine its Fracture Mechanism and Strain Rate Sensitivity
Micropillar Compression Testing with In-situ Raman Spectroscopy to Study Plastic Deformation in Vitreous Silica
Microstructure-driven Mechanical Properties of Explosives Quantified with In-situ Tomography
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Microtensile Testing of (fcc) Copper and (hcp) Titanium at Elevated Temperatures
Mixed-mode Fracture Behavior of Magnesium Alloys
Multiscale Modeling to Determine Bulk Material Property from Miniature Specimen Testing
Numerical Study of Plastic Deformation Mechanisms in a New Generation Fe-TiB2 Steel Composite Using a FFT-based Model
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Quantifying Deformation Mechanics of High Temperature Alloys using In-situ and Digital Imaging Correlation (DIC) Testing Techniques
Shape Fidelity and Mechanical Response in Micro Pattern Replication by Molding
Synchronized Indentation and Raman Spectroscopy for Crystal Engineering
Synthesis and Mechanical Behavior of Freestanding NiTi Films with Varying Grain Sizes
Temperature Effects in the Microscale Deformability of Yttria Stabilized Zirconia Prepared by Spark Plasma Sintering
Understanding Pseudomorphic bcc Mg Under Extreme Conditions of Pressure, Temperature and High Strain Rates

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