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Meeting MS&T21: Materials Science & Technology
Symposium 2021 Undergraduate Student Poster Contest
Presentation Title Rheological Characterization of Highly Loaded Alumina-Polymer Suspension for Thermal Paste 3D Printing
Author(s) Pattiya Pibulchinda, Caitlin Adams, Kendra Erk
On-Site Speaker (Planned) Pattiya Pibulchinda
Abstract Scope Thermal interface material (TIM) pastes are thermally conductive fillers in a polymer matrix to transfer heat. The liquidity of thermal paste causes dripping defects at the end of 3D printed lines. This study investigated the influence of rheological factors on TIMs flow behaviors in direct ink 3D printing. Highly loaded alumina-polymer suspensions were formulated by varying the volume percentage of alumina powder and polyvinylpyrrolidone (PVP) polymer. Key rheological properties are yield stress, viscosity-shear rate dependency, cohesive strength, and shear strain retraction during creep cycles. Printing and dripping issues were identified as several 3D printing speeds and setup changes. Commercial alumina-based TIM tails more continuously while the formulated suspensions drip discretely in drops. This research developed rheometric experimental procedures to simulate TIM behavior in the 3D printing process. By applying constant shear stress cycles in the rheometer, the shear strain and viscosity behavior in direct ink 3D printing were successfully characterized.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Composition and Physicochemical Properties of Typical Waste Cooking Oil
Effect of Carbon Stoichiometry on the Heat of Formation of Hafnium Carbides
Effect of Modifier Cation Size on the Bulk Structure and Nickel Speciation in Alkali Borosilicate Glasses
Electron Cloud Migration Effect-induced Lithiophobicity/Lithiophilicity Transformation for Dendrite-free Lithium Metal Anodes
Enhanced Mechanical Properties in a 4140 Steel by "In-House" Intensive Quench
Experiential Study on Critical Stress Intensity Factor of Carbon Nanotube Filled Epoxy
Exploring the Liquid Phase Exfoliation of Two-Dimensional Bilayered Vanadium Oxide in Aqueous Media for Li ion Batteries
High Temperature Mechanical Properties of TiB2-WC-SiC Materials
Highly Crystallized Prussian Blue with Enhanced Kinetics for Highly Efficient Sodium Storage
Investigation of Embedded Metallic Components on 3D Printed Ceramic Structures
Machine Learning Approaches to Predict Properties from Microstructure Images in Ceramic-Metal Composites
Mechanical Behavior of Automotive Structural Steels in the Vicinity of the Ductile-brittle Transition
Mechanical Property Assessment of Silicon Carbide Fiber-reinforced Epoxy-matrix Composites
Optimal Integration of TiO2-Coated Gold Nanostars for Enhancement of Photocatalytic Water Reduction
Perovskite Film Formation for Solar Cell Absorbers: Effects of Substrate Modification
Pressure Optimization of Fast-Moving Silicon MEMS Micromirrors
Processing and Properties of (Ta, Nb, Hf, Ti)C
Rheological Characterization of Highly Loaded Alumina-Polymer Suspension for Thermal Paste 3D Printing
The Dynamic Performance of Wearable Sensors with Flexible Silver Ink
The Mechanisms of Micro-fine Titanaugite Enter to Ilmenite in the Flotation and Depression Behavior of Sodium Silicate
Thermal Analysis of Sodalite-immobilized Iodine-129 Caustic Scrubber Slurry
ZrB2 Aqueous Slurry Development for DIW Additive Manufacturing

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