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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Advances in Surface Engineering VIII
Presentation Title Fabrication of a Highly Stable and Sensitive Iridium Oxide Nano-Needle pH Sensor Using Electrochemical Deposition
Author(s) Kyu Hwan Lee, Min-Yeong Kim
On-Site Speaker (Planned) Kyu Hwan Lee
Abstract Scope Iridium Oxide Nano-Needles (IrOx NNs) were synthesized using a simple electrochemical deposition method and integrated onto a Screen-Printed Carbon Electrode (SPCE) to develop a novel pH sensor. The nano-needle structure was controlled by adjusting the annealing temperature, with optimal morphology achieved at 650 °C. This unique structure enhanced the surface area and electron transfer, leading to improved sensor performance. The fabricated sensor, using a two-electrode system with an Ag/AgCl reference, showed a near-Nernstian response of 58.27 mV/pH over a wide pH range (2–12) at 25 °C. Surface chemistry was analyzed by XPS, and the active surface area was evaluated electrochemically. The sensor demonstrated excellent sensitivity, stability, response time, reproducibility, and selectivity, highlighting the strong potential of IrOx NNs for advanced pH sensing applications.
Proceedings Inclusion? Planned:
Keywords Surface Modification and Coatings, Thin Films and Interfaces,

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Effect of Nanoparticles on the Anodization of Aluminum Alloys
Enhanced Durability of Refractory High-Entropy Alloys via Laser-Induced Periodic Surface Structures
Fabrication of a Highly Stable and Sensitive Iridium Oxide Nano-Needle pH Sensor Using Electrochemical Deposition
In-Situ Solid State Method for Fabricating Functionally Multilayered Yb-Silicate Environmental Barrier Coatings
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Nanosecond Laser-based Surface Engineering for Extreme Wettability-driven Long-term Corrosion Protection of Aluminum Alloys
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