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Meeting 2027 TMS Annual Meeting & Exhibition
Symposium AI-Enabled Materials Processing: Integrating Accelerated Experimental Workflows and Processing-Aware Machine Learning
Presentation Title Closed-loop machine learning guided exploration of processing pathways reveals optimal microstructures
Author(s) Sreenivas Raguraman, Maitreyee Sharma Priyadarshini, Andrew Kim, Tunde Ayodeji, Veronica Ivanovskaya, Beril Ulugun, Camryn Byrum, Adam Griebel, Paulette Clancy, Timothy Weihs
On-Site Speaker (Planned) Sreenivas Raguraman
Abstract Scope AI-enabled materials design often emphasizes composition- or microstructure-based descriptors, but practical materials development requires processing pathways that can be experimentally implemented and can reliably produce targeted combinations of properties. Here, we demonstrate a closed-loop, processing-aware machine-learning workflow to optimize thermomechanical pathways in a fixed-composition ZX10 magnesium alloy. Processing descriptors spanning strain, heat-treatment temperature, duration, and sequence were used as model inputs, while hardness and corrosion rate served as rapid experimental feedback signals. Across three experimental rounds, the workflow evolved from a broad property-ratio search to a multi-objective, feasibility-informed strategy that identified implementable pathways with improved hardness and reduced corrosion. Post-optimization characterization shows that the best-performing pathways converged toward a common microstructural state consisting of ultrafine grains, comparable defect densities, similar texture, and finely distributed precipitates, even without microstructural input. These findings show that processing-aware machine learning can guide processing toward favorable microstructural states without requiring microstructural inputs during optimization.
Proceedings Inclusion? Planned:
Keywords Machine Learning, Process Technology, Biomaterials

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