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Meeting 2027 TMS Annual Meeting & Exhibition
Symposium Spectroscopic Methods and Analysis for Nuclear Energy Related Materials
Presentation Title Understanding Temperature in Extreme Conditions
Author(s) Tiffany Y. McHenry, Donald Brown, Matthew Kerr, Don Lipkin
On-Site Speaker (Planned) Tiffany Y. McHenry
Abstract Scope Accurate temperature measurement of high-temperature materials remains a fundamental challenge in thermal metrology due to the inherent coupling between emissivity and temperature in pyrometric measurements. Since most real materials exhibit non-gray behavior, the gray-body emissivity assumption can introduce significant uncertainty in brightness temperature measurements. This work investigates spectroscopic approaches for the simultaneous determination of temperature and emissivity through optimization of physically constrained emissivity models that require no prior knowledge of a material's emissivity. Spectral radiance measurements acquired over a broad wavelength range are analyzed using Planck-based radiative transfer models coupled with parameterized emissivity representations for well-characterized materials. Temperature estimates obtained from spectroscopic measurements will be independently validated through X-ray diffraction (XRD) at the synchrotron, where lattice parameters will be measured and correlated with temperature using established thermal expansion relationships. By combining spectroscopic diagnostics with diffraction-based thermometry, this methodology aims to improve temperature accuracy for non-gray materials in extreme environments.
Proceedings Inclusion? Planned:
Keywords Phase Transformations, High-Temperature Materials, Modeling and Simulation

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advancing Neutron Scattering Techniques for Nuclear Materials
Application of Synchrotron X-ray Absorption Spectroscopy to Nuclear Materials
Characterizing Nuclear Energy Related Materials with Laser Ablation Laser Ionization (LALI) Mass Spectrometry
Chemical bonding in UO3 polymorphs: a QTAIM–Hessian-matrix perspective on short U–O and oxo bonds
Determination of High Temperature Mechanical Properties of Nuclear Fuel Using Temperature Resonant Ultrasound Spectroscopy
High temperature Raman spectroscopy of in-situ annealing of ion irradiated SiC and residual stresses in SiC/SiC composites
In-situ Raman Spectrometry of Passive Surface Layers on Stainless Steel
In-Situ UV–Vis Quantification of Chlorobasicity in Binary Molten Chlorides: A Spectroscopic Framework for Molten Salt Reactor Chemistry
Irradiation-damage Response of Stable Grain-boundary-decorated Nanocrystalline Multi-principal-element Alloy
Linking Atomic Structure to Engineering Performance in Refractory Materials for Fusion and Fission
Multimodal chemical imaging and microanalysis of intermetallic materials
NMR Spectroscopy of Zirconium Carbides after High-Temperature Hydrogen Exposure
Nuclear Materials Research using the Activated Materials Laboratory and the Advanced Photon Source
One dislocation, one pore at a time: Probing radiation damage in nuclear materials
Potential of atom probe tomography for mapping hydrogen isotopes in nuclear materials
Raman Spectroscopy of Lanthanides in LiCl-KCl Eutectic for Nuclear Energy Systems
Real-Time Spectroscopic Characterization of Molten Salt Systems Using Electrochemical–LIBS Data Fusion and Probabilistic Neural Networks
Surface-Sensitive X-ray Absorption Spectroscopy for Investigating Corrosion Mechanisms in Actinide Metals
Synchrotron-based high-{energy/temperature/strain/modality} characterization resources for nuclear materials research at NSLS-II
Three-Dimensional Characterization of Crack and Inclusion Networks in a Service-Exposed Baffle Former Bolt Using High-Energy X-Ray Microscopy
Understanding Temperature in Extreme Conditions

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