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Meeting MS&T25: Materials Science & Technology
Symposium Emergent Materials Under Extremes and Decisive In Situ Characterizations
Presentation Title In-Situ Neutron Diffraction-Based Creep Evaluation of Co- and Ni-Based Superalloys Produced by Laser Powder Bed Fusion
Author(s) Noah Holtham, Patxi Fernandez-Zelaia, Frank Brinkley, Christopher Fancher, Christopher Ledford, Ning Zhou, Stéphane Forsik, Tresa Pollock, Michael Kirka
On-Site Speaker (Planned) Noah Holtham
Abstract Scope In this work, recently developed high γ’ alloys designed for laser powder bed fusion (LPBF) processing, GammaPrint®-700 (Co-based) and GammaPrint®-1100 (Ni-based), were subjected to creep testing while being continuously monitored via the VULCAN instrument at the ORNL Spallation Neutron Source to measure the phase-specific strain behavior and deformation mechanisms in-situ. Specimens from both alloy systems were subjected to thermomechanical loads of 760 °C/500 MPa and 900 °C/175 MPa for 10 hours or until rupture. Diffraction data showed that the ordered γ’ phase accommodated most of the tensile strain while the surrounding γ matrix compressed due to the lattice parameter and stiffness mismatch. SEM, EDS, and EBSD analysis revealed small differences in phase fraction, texture, solute partitioning which were determined to be minor contributors to the creep behavior. The in-situ creep testing of GammaPrint®-700 and GammaPrint®-1100 alloys demonstrates the significant potential of LPBF-optimized Co–Ni superalloys in high temperature applications.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Approaches to Functional High-Pressure Phases: Pressure Aging and Structural Mimicry
Assessment of Defects in AlGaN Induced by High Electronic Excitations Using Ionoluminescence and RBS Channeling
Characterization of Phase Transformations in Oxides Driven by Far-From-Equilibrium Conditions
Deployment and Testing of a Fiber-based Instrument for In-reactor Thermal Property Measurements at MIT Research Reactor
Dynamic behavior of porous materials under shock loading
Emergent Material Characterization by Synchrotron-Based X-ray Imaging, Spectroscopy and Scattering
Exploring Catalytic Pathways Using Advanced X-Ray Spectroscopy Techniques
High Temperature Creep, Plasticity and Failure; New Insights from In Situ TEM
In-Situ Characterization of High-Temperature Degradation of Nuclear Materials under Extreme Environments
In-Situ Neutron Diffraction-Based Creep Evaluation of Co- and Ni-Based Superalloys Produced by Laser Powder Bed Fusion
In Situ Characterization of Rare Earth Element Complexation and Crystallization Pathways in Hydrothermal Fluids under Extreme Conditions
In Situ Ion Irradiation of Uranium Carbide
In Situ Tomography Testing in Extreme Environments
Metal Fuel Performance in Sodium-Cooled Fast Reactors: Post Irradiation Examination
Pressure-induced changes in the density and local structure of GeO2 glass under high pressure
Quantifying Micromechanical Behavior of Fe-36Ni Invar Alloy in Low-Temperature Conditions using 3D X-ray Diffraction
Studies of quantum materials under high pressure

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