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Meeting MS&T25: Materials Science & Technology
Symposium Engineering Ceramics: Microstructure-Property-Performance Relations and Applications
Presentation Title Hybrid Microwave Sintering of Electrolytes for SOEC/SOFC Applications
Author(s) Tugrul Yumak, Mohan Thorat, Ansan Pokharel, Javier Mena, Katarzyna Sabolsky, Shavinka Jayasekera, Terence Musho, Edward Sabolsky
On-Site Speaker (Planned) Tugrul Yumak
Abstract Scope Doped-Zirconia and -ceria ceramics are the most widely used electrolytes in solid oxide fuel cells (SOFCs) and solid oxide electrolysis cells (SOECs) due to their high oxygen-ion conductivity, chemical stability, and mechanical strength at elevated temperatures. Conventional densification of YSZ (Y-stabilized zirconia) typically requires sintering at 1350–1550°C for 2–5 hours, with a heating rate of 2–5°C/min and a cooling rate of 1–3°C/min. However, this process is highly time-consuming and energy intensive. From an economic standpoint, hybrid microwave (MW) sintering, which enables densification within 20–25 minutes, presents a promising alternative.We investigate the influence of key MW processing parameters on the physical, microstructural, and electrochemical properties of YSZ and other electrolyte materials. A comparative analysis with conventionally sintered materials was conducted to evaluate the effectiveness of hybrid MW sintering. In addition, electrochemical impedance spectroscopy (EIS) and conductivity measurements were conducted to discuss the final electrochemical properties.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Statistical Model of Microstructural Toughening in Ceramics
Breaking the Charge Neutrality Boundary in Perovskite Using the PyCALPHAD Approach
D-14: Effects of Electrode and Substrate Optimization on Solid Oxide Cell Performance
Design and Sintering of Ceramic-Metal Composites for Extreme Environment Applications
Development of a Li-Corrosion Resistant Coating for Mullite-Cordierite-Based Refractory
Effect of Carbon on the Microstructure and Phase Evolution of High Entropy Dual Phase Ceramics
Effect of SiO2 Content on High-Temperature Phase Transition and Physical Properties in Calcium Aluminate Cement
Fatigue Behavior of Grain Boundaries in High Thermal Conductivity Silicon Nitride Ceramics Evaluated by Microcantilever Bending Test
Finite Element Modeling of Microwave-Assisted Calcination of SOEC Perovskite Precursor Powders
Firing Behavior of 18th Century European Porcelains
Hybrid Microwave Sintering of Electrolytes for SOEC/SOFC Applications
Measurement of Glaze Thermal Expansion via Crazing
Microstructure Development of Electro-Conductive Aluminum Nitride for Sensor Applications
Percolation-Driven Thermal Conductivity Improvement in Pyrolyzed MXene/SiOC Nanocomposites
Reduction Behavior of Mullite/Andalusite-Based Refractories Under Hydrogen Atmosphere and the Effect of Crystalline SiO2 on Mechanical Strength
Small Tests that Make a Big Difference: Correction of the Plastic Size Effect During Micromechanical Testing

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