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Meeting MS&T25: Materials Science & Technology
Symposium Advances in Refractory High Entropy Alloys and Ceramics
Presentation Title Mechanisms of spall failure in niobium subjected to high-throughput laser-driven micro-flyer impact
Author(s) Nicolo Della Ventura, Arezoo Zare, Jacob Diamond, Todd Hufnagel, K.T. Ramesh, Daniel S. Gianola
On-Site Speaker (Planned) Nicolo Della Ventura
Abstract Scope Designing BCC alloys for shock resistance requires understanding microstructural evolution and failure mechanisms under dynamic loading. However, conventional plate impact experiments are time-consuming and costly, and the deformation behavior of pure BCC metals remains poorly understood. To address this, a high-throughput laser-driven micro-flyer technique was used to study spall failure in pure niobium at strain rates of 10⁶ 1/s and peak shock stresses between 7.3 and 15.3 GPa. Post-mortem analysis of samples recovered at incipient and advanced failure states reveals ductile failure through mixed intergranular and intragranular fracture. Cavities nucleating within grains grow via dislocation emission from void surfaces until a radius of approximately 260 nm, after which cracks propagate along {101} planes. Misorientation gradients and high-angle grain boundaries at crack fronts indicate dynamic recrystallization in heavily deformed regions. The observed spall strengths and microstructural features are discussed in relation to analytical models of cavitation-driven failure.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advancements and Challenges in Electron Beam Powder Bed Fusion of Refractory Alloys
AI-Driven Discovery of Compositionally Complex Alloys for Enhanced Mechanical Performance
Commercial Alloys Through a High-Entropy Lens
Composition design of refractory compositionally complex alloys using machine learning models
Creep Behavior of a Precipitation-Strengthened A2-B2 Refractory High Entropy Alloy
Design, Synthesis, and Properties of WTaCrVHf High Entropy Alloys
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Exploring the thermodynamic stability of the high entropy ultra-high temperature ceramic composition space (Ti,Zr,Hf,Nb,Ta)C1-x
Heat Transport in WMoTaNbV High-Entropy Alloy via First-principles Calculation
High-Entropy Oxides and Halides: Expanding the Energy-Materials Space
High-Temperature Mechanical Behavior of Refractory Alloys
Improving the Use of Machine Learning Tools for High Entropy Alloy Development
Mechanisms of spall failure in niobium subjected to high-throughput laser-driven micro-flyer impact
Microstructure, Micromechanical and Thermal Properties of Irradiated High Entropy Carbide Ceramics
Multi-Modal Characterization of the B2 Phase in the Ta-Re Binary System
Multiphase Design Strategies in Nb–Ti Refractory Alloys with Interstitial Alloying
On the Strength and Ductility of Refractory High Entropy Alloys
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Refractory High-Entropy Borides, Nanoalloys, and Dual-Phase Composites with a Broader Perspective
Refractory High Entropy Alloys in Extreme Environments
Selective laser sintering and spark plasma sintering of compositionally complex carbide ceramics
Simulations and modelling of the mechanical behavior of compositionally complex concentrated BCC alloys
Tailoring Nb-Ti-Si-B RCCA Microstructures by Modeling and Thermomechanical Processing
Tensile Creep Mechanisms of the Nb45Ta25Ti15Hf15 and NbTaTiV Refractory High-Entropy Alloys
Thermal conductivity of high entropy ceramics before and after irradiation
Thermal Control During Laser Powder Bed Fusion of Pure Tungsten Through Optimization of Follower Beam
Tuning Chemical Short-Range Ordering and Mechanical Properties in a Ductile Refractory Multi-Principal-Element Alloy
Two-shot Optimization of Compositionally Complex Refractory Alloys
ULTERA Data Ecosystem for Compositionally Complex Materials
Ultrasonic atomization of a hafnium based refractory high-entropy alloy Ti20Zr20Nb20Hf20Ta20
Understanding Compositional and Structural Non-uniformities in Refractory High Entropy Alloys

Fundamental Property Measurements of Fully Dense (Cr,Mo,Ta,V,W)C1–x High-Entropy Carbide Ceramic


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