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Meeting MS&T25: Materials Science & Technology
Symposium Emergent Materials Under Extremes and Decisive In Situ Characterizations
Presentation Title In Situ Tomography Testing in Extreme Environments
Author(s) Alex G. Arzoumanidis
On-Site Speaker (Planned) Alex G. Arzoumanidis
Abstract Scope Rotating the load train within a mechanical load frame provides enables extreme in-situ testing during X-ray computed tomography (CT) scans. It also introduces substantial alignment challenges. CT reconstruction algorithms require rotation about an axis with minimal deviation or runout, a problem exacerbated by the dual rotation stages required by rotating load train systems. A careful mechanical design limits vertical and horizontal runout on a 10kN system is kept to less than one micron. A four degree of freedom fixture aligns the two axes to each other, which is particularly important for longer load trains, often needed to insulate the load cell and actuator from extreme sample temperature. A convective current environmental chamber capable of CT from -60C to 300C is discussed, as well as a 1600C furnace, whose novel control algorithm can control temperature to 0.1C. The rotating load train also facilitates laser heating to temperatures beyond 1600C.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Approaches to Functional High-Pressure Phases: Pressure Aging and Structural Mimicry
Assessment of Defects in AlGaN Induced by High Electronic Excitations Using Ionoluminescence and RBS Channeling
Characterization of Phase Transformations in Oxides Driven by Far-From-Equilibrium Conditions
Deployment and Testing of a Fiber-based Instrument for In-reactor Thermal Property Measurements at MIT Research Reactor
Dynamic behavior of porous materials under shock loading
Emergent Material Characterization by Synchrotron-Based X-ray Imaging, Spectroscopy and Scattering
Exploring Catalytic Pathways Using Advanced X-Ray Spectroscopy Techniques
High Temperature Creep, Plasticity and Failure; New Insights from In Situ TEM
In-Situ Characterization of High-Temperature Degradation of Nuclear Materials under Extreme Environments
In-Situ Neutron Diffraction-Based Creep Evaluation of Co- and Ni-Based Superalloys Produced by Laser Powder Bed Fusion
In Situ Characterization of Rare Earth Element Complexation and Crystallization Pathways in Hydrothermal Fluids under Extreme Conditions
In Situ Ion Irradiation of Uranium Carbide
In Situ Tomography Testing in Extreme Environments
Metal Fuel Performance in Sodium-Cooled Fast Reactors: Post Irradiation Examination
Pressure-induced changes in the density and local structure of GeO2 glass under high pressure
Quantifying Micromechanical Behavior of Fe-36Ni Invar Alloy in Low-Temperature Conditions using 3D X-ray Diffraction
Studies of quantum materials under high pressure

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