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Meeting 2027 TMS Annual Meeting & Exhibition
Symposium Next Generation Electrometallurgical Technologies for Metal Extraction, Refining, and Recycling
Presentation Title Recovery of Valuable Metals From Secondary Resources Using Molten Oxide Electrolysis
Author(s) Dongjin Han, Joongseok Kim, Jungshin Kang
On-Site Speaker (Planned) Jungshin Kang
Abstract Scope In this study, molten oxide electrolysis (MOE) using a Na2O–B2O3 electrolyte was investigated to recover valuable metals, including Ni, Co, Zn, and Fe, from industrial wastes. For Ni and Co recovery from residues generated during spent desulfurization catalyst recycling, the effects of applied voltage in the range of 0.6–1.2 V and electrolyte composition were examined at 1173 K. Using Pt electrodes, Ni and Co were preferentially electrodeposited at 0.6 V, and the cathode surface contained 29.0 mass% Ni and 5.26 mass% Co. The applicability of MOE to Fe and Zn recovery from EAF dust was also examined at 1173 K. Applied voltage and feed composition affected the electrochemical reduction behavior, enabling selective Fe reduction at 1.1 V or co-reduction of Fe oxide and ZnO at 1.6 V. These results demonstrate the feasibility of MOE for recovering valuable metals from complex oxide-bearing secondary resources.
Proceedings Inclusion? Planned:

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Electrons as Reductants: Transforming Metal Production through Electrometallurgy
Engineering Transition Metal Oxide Electrode for Direct Lithium Extraction from Aqueous Brines
Evidence of Silicon Production from Fluxed End-of-Life Photovoltaic Glass via Molten Oxide Electrolysis
High-Temperature Molten Salt Electrolysis for Sustainable Small-Molecule Chemical Synthesis
Liquid-Metal Bipolar Membrane for Electrochemical Recovery of Critical Metals in Molten Salts
Molten Salt Electrolysis for Iron Production: Progress Toward Decarbonized Ironmaking
Nordic Salt Cycle – Scaling a Molten Salt Process for Critical Mineral Recovery to Pilot
Recovery of Valuable Metals From Secondary Resources Using Molten Oxide Electrolysis
Thermodynamic and Experimental Investigation of In-Furnace Recycling of Electric Arc Furnace Dust
Three-Layer Electrorefining of Liquid Zn and Pb Held on/in Porous Holding Materials in Molten Chlorides

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