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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Advances in Thermo-Mechanical Processing of Refractory Alloys
Presentation Title Influence of Thermo-Mechanical Processing on Microstructure and Mechanical Behavior of HfTiZrNbx Alloys
Author(s) Joseph Tamirka Bawah, Peter K. Liaw, Eric. A. Lass
On-Site Speaker (Planned) Joseph Tamirka Bawah
Abstract Scope Refractory high-entropy alloys, BCC-structured, offer promising strength and stability for advanced high-temperature applications. This study investigates the effect of thermal processing and Nb content on the microstructure and mechanical behavior of HfTiZrNbx (x = 0.3 - 0.8) alloys. The as-cast alloys possess single-phase BCC microstructures and exhibit strengths exceeding 1000 MPa. However, ductility is limited to ~14 % for x > 0.5 and even less for x < 0.5. Homogenization at 1200°C retains the BCC structure, but strength is decreased considerably. Ductility is improved considerably with tensile elongations of >10 % for x < 0.5 alloys. Aging at 725°C promotes the precipitation of a second phase, HCP, and brittle behavior is observed. For alloys with x < 0.5, the brittle behavior is attributed to the presence of the HCP precipitates, while intergranular failure is the cause of failure for alloys with x > 0.5.
Proceedings Inclusion? Planned:
Keywords High-Entropy Alloys, Mechanical Properties, Phase Transformations

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Breaking the Brittleness Barrier: How Severe Plastic Deformation and Interstitials Affect Plasticity in the TaNbVZrTi RHEA
Controlling Interstitial Impurities to Enable Conventional Manufacturing of Refractory Multi-Principal-Element Alloys
Design of ruthenium containing BCC+B2 refractory alloys and their deformation behavior
Dislocation mechanisms governing the continuous and discontinuous dynamic recrystallization behavior in refractory multi-principal element alloys
Effect of varied thermomechanical processing and heat treatment strategies on MoNbTi
High ductility in as-sintered Mo produced by pressureless sintering
Influence of Combined Thermal and Mechanical Processes on the Recrystallization of Ta–W Alloys
Influence of Thermo-Mechanical Processing on Microstructure and Mechanical Behavior of HfTiZrNbx Alloys
Investigation of microstructure evolution during spin forming of a tantalum-tungsten alloy
Investigation of Oxidation Resistance and Hot Deformation Behaviour of Refractory Al0.2 Cr0.2Mo0.2Nb0.2Ta0.2 High-Entropy Alloy Synthesized by Adiabatic Aluminothermic Process
Ordering induced enhancement of mechanical properties of NbTaTi equiatomic RCCA
Phase Field Modeling of {110} and {112} Slip in W-Re Alloys
The thermal mechanical behavior of refractory alloys at extreme temperatures
Thermomechanical processing of ductile refractory alloys: An industrial perspective
Towards the Production of Bulk Ultra Fined Grained Ductile Tungsten

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