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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Novel Strategies for Rapid Acquisition and Processing of Large Datasets From Advanced Characterization Techniques
Presentation Title Nanocrystalline Films: Imaging, Orientation Mapping, Machine Learning and Data Analytics
Author(s) Katayun Barmak, Jeffrey Rickman
On-Site Speaker (Planned) Katayun Barmak
Abstract Scope The interrogation of nanometer-scale thin-film microstructures requires the use of scanning/transmission electron microscopy (S/TEM). Advances in low thermal mass holders, MEMS chips for film deposition onto electron transparent membranes, and in-situ heating capabilities combined with drift correction have revolutionized our ability to image grain growth in real time. Additionally, grain-boundary crystallography and character distribution (GBCD) of nanocrystalline films can now be obtained using precession electron diffraction (PED) 4D-STEM. Thin films therefore offer a unique platform for accessing both direct space (imaging) and reciprocal space (orientation mapping) at high spatial/temporal resolution. This talk will summarize how innovations in automated boundary detection of bright-field TEM images using machine learning (ML) followed by analysis of the imaging and mapping data provide unprecedented ability to deepen our understanding of grain growth. In this context, ML is employed to reconstruct grain-boundary networks, quantify the rate of microstructural learning and inform coarsening models with experimental data.
Proceedings Inclusion? Planned:
Keywords Characterization, Thin Films and Interfaces, Machine Learning

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Advancements in Titanium Microstructure Characterization: Integrating AI for Automated Complex Quantification
Advances in Analytical S/TEM-Based Workflows: Emerging Techniques for Smarter Data Acquisition and Processing
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Advancing Segregation Characterization in Steel and Alloys: A Novel BEX-EDS-SEM Approach
Affine Transformations to Correlate Experimental and Simulated EDS Spectra for Multi-Element Systems
Automated 2D Microscopy Workflows for Multimodal Characterization of Structure, Crystallography and Composition
Comprehensive Microstructural Characterization of Aging-Treated Aluminum Alloy AA2024 Using Integrated SEM, STEM, EDS, and EBSD Workflows
Conditional Diffusion Models for Microscopy Modality Transfer of Electron Backscattering Microscopy Diffraction Misorientations Maps from Optical Microscopy
Discovering Hidden Fingerprints in Multimodal Process-Structure-Property Data via Joint Embedding
Emphasizing the Importance of Data Exchange in Constructing a Digital Twin for Metals-AM
Enabling Data Starved Microstructural Segmentation With Foundation Models as First-Pass Segmentors in Low-Contrast Al-Si Solidification
Examining Growth Twinning in Ni-Based Films via a High-Throughput Methodology
Frequency-Domain Thermoreflectance Automation for High Throughput Microstructural and Thermal Characterization
High-Throughput Crystallography by Quantitative Large-Area Polarized-Light Microscopy
High-Throughput Exploration of Large Material Design Spaces Using Small Samples and Bayesian Strategies
High-Throughput Processing and Accelerated Characterization of Cu–Ti Alloy
High-Throughput Time-Resolved X-Ray Computed Tomography to Characterize Flaw Evolution in LPBF Parts During Creep
High Throughput Texture Analysis of Quartz via Automated Polarized Reflective Light Microscopy
Increasing the Throughput of Ultra-High Temperature Ceramic Tensile Testing
Lightweight Services and Federated Storage for Data-Intensive Structural Materials Research
Linking Energetic Material Sensitivity and Microstructure Variability Across Length Scales
Machine Learning Assisted Structure-Property Relationships by Nanoindentation
Mapping Microstructure to Field Properties in Materials Under Dynamical Loading
Nanocrystalline Films: Imaging, Orientation Mapping, Machine Learning and Data Analytics
New Strategy of Surface Defect Detection in Metallic Coatings Using a Machine Learning-Based Model
Same-Day Product Quality Assessment of CaCl₂-Assisted Direct Reduction of Chromite via µCT and Deep-Learning Segmentation Against a Reference Dataset
Segmentation Methods for Tracking Dislocation Dynamics

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