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Meeting MS&T25: Materials Science & Technology
Symposium Emergent Materials Under Extremes and Decisive In Situ Characterizations
Presentation Title In-Situ Characterization of High-Temperature Degradation of Nuclear Materials under Extreme Environments
Author(s) Di Chen
On-Site Speaker (Planned) Di Chen
Abstract Scope High-temperature environments pose significant challenges for studying material degradation, particularly in capturing thermal transport behavior and microstructural evolution under simultaneous irradiation and heating. We present an advanced in-situ characterization platform designed to address these challenges. The system combines localized laser heating, infrared thermography, and numerical modeling to extract spatially resolved thermal conductivity and emissivity in real time. Under 700 keV ion irradiation, the platform reveals clear fluence-dependent reductions in thermal conductivity near the surface—offering a rapid alternative to traditional ex-situ techniques. To further support research under extreme thermal conditions, a new infrastructure has been established, featuring a precision-controlled heating stage capable of reaching 1500°C, in-situ optical microscopy, and Raman spectroscopy. This setup enables continuous monitoring of structural changes during high-temperature exposure and irradiation. Together, these capabilities provide critical insights into material degradation mechanisms and support the accelerated development and qualification of advanced materials for demanding environments.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Approaches to Functional High-Pressure Phases: Pressure Aging and Structural Mimicry
Assessment of Defects in AlGaN Induced by High Electronic Excitations Using Ionoluminescence and RBS Channeling
Characterization of Phase Transformations in Oxides Driven by Far-From-Equilibrium Conditions
Deployment and Testing of a Fiber-based Instrument for In-reactor Thermal Property Measurements at MIT Research Reactor
Dynamic behavior of porous materials under shock loading
Emergent Material Characterization by Synchrotron-Based X-ray Imaging, Spectroscopy and Scattering
Exploring Catalytic Pathways Using Advanced X-Ray Spectroscopy Techniques
High Temperature Creep, Plasticity and Failure; New Insights from In Situ TEM
In-Situ Characterization of High-Temperature Degradation of Nuclear Materials under Extreme Environments
In-Situ Neutron Diffraction-Based Creep Evaluation of Co- and Ni-Based Superalloys Produced by Laser Powder Bed Fusion
In Situ Characterization of Rare Earth Element Complexation and Crystallization Pathways in Hydrothermal Fluids under Extreme Conditions
In Situ Ion Irradiation of Uranium Carbide
In Situ Tomography Testing in Extreme Environments
Metal Fuel Performance in Sodium-Cooled Fast Reactors: Post Irradiation Examination
Pressure-induced changes in the density and local structure of GeO2 glass under high pressure
Quantifying Micromechanical Behavior of Fe-36Ni Invar Alloy in Low-Temperature Conditions using 3D X-ray Diffraction
Studies of quantum materials under high pressure

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