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Meeting MS&T24: Materials Science & Technology
Symposium Advanced Manufacturing of High Temperature Ceramics and Composites: Processing, Characterization and Testing
Presentation Title Robocasting SiC Using Sub-mm Nozzle Sizes
Author(s) Josh Robinson, Cooper Howard, Yuxuan Sun, Scott Misture
On-Site Speaker (Planned) Scott Misture
Abstract Scope SiC pastes were optimized for pressureless sintering at 2200C or lower temperatures and then further optimized to enable reliable 3-D printing using Hyrel extrusion printers. Sintering aids and additives were limited to small fractions in order to produce SiC that is both >95% dense and applicable for ultrahigh use temperatures. Pastes were optimized for 0.6 and 1.0 mm nozzle sizes, and parts were produced on the size scale of 8 by 8 by 2 cm tall using single-layer and as many as 4-layer wall thicknesses. Complex shapes that mimic wing leading edges and similar aerospace-relevant components have been produced by printing the optimized pastes, followed by controlled-humidity drying, and finally sintering in graphite crucibles at temperatures ranging from 2100 to 2200C. We demonstrate that crack-free drying is of critical importance, as is preparing the pastes using traditional and/or non-traditional methods for reducing agglomeration and improving mixedness.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A-13: Comparing the Measured Permittivity with the Mixing Rules of Maxwell-Garnett, Bruggeman, and the Coherent Potential
A-14: Hyperdoping: Doping TiO2 Beyond Thermodynamic Limits Using Flash Sintering
A-15: Optimization of Ball Milling and Spark Plasma Sintering Process Parameters for Graphene Nanoplatelets Reinforced IN718 Composites
Additive Manufacturing of Carbon Fiber Reinforced Ceramic Matrix Composites (C/C-SiC)
Additively Manufactured Reaction Bonded Porous Silicon Nitride
Advanced Manufacturing of PIP-Based SiC-SiC CMCs
Advanced Silicon Carbide Fabrication Using Laser Induced Slip Casting
Novel Joining of Ceramic Matrix Composites Using Embedded Wire Heating and Chemical Vapor Deposition (EWCVD)
Optimization and Considerations for the Fabrication of Highly Loaded Chopped Carbon Fiber Reinforced SiC Matrix Composites Through Direct Ink Writing and Silicon Melt Infiltration Processes
Optimizing Solids Loading for Aqueous Robocasting of Monolithic Silicon Carbide
Reactive Melt Infiltration Approaches for Ultra-High Temperature Ceramic Composites
Robocasting SiC Using Sub-mm Nozzle Sizes
Synthesis and Characterization of Next-Generation Multiphase Silicon Nitride-Based Structural Ceramics
Thermal Properties of Oxidized and Non-Oxidized 2D Pitch-Based and 3D PAN-Based C/C Composites

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