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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Dilute Alloying and Impurity Effects on Phase Transformations
Presentation Title Dopant-Driven Grain Boundary Segregation in High Entropy Alloy Nanoparticles
Author(s) Daniela P. M. Fonseca, Ricardo H. R. Castro, Martin P. Harmer
On-Site Speaker (Planned) Daniela P. M. Fonseca
Abstract Scope Controlling microstructure evolution during sintering is critical to unlocking the full potential of high entropy alloy (HEA) nanoparticles for powder-based manufacturing. Yet, the role of dopant elements in driving atomic-scale transformations during thermal processing remains largely unexplored. In this work, we investigate HEA nanoparticles synthesized via fast moving bed pyrolysis (FMBP), with dilute additions of alloy elements. Using in situ heating transmission electron microscopy (TEM) coupled with energy-dispersive X-ray spectroscopy (EDS), we aim to determine whether these dopants induce chemical disorder within individual nanoparticles, promote segregation at grain boundaries, and influence overall densification behavior. These findings offer insights into how controlled minor alloying can be leveraged to tailor sintering kinetics and guide microstructure evolution in HEA systems.
Proceedings Inclusion? Planned:
Keywords High-Entropy Alloys, Phase Transformations, Powder Materials

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Anomalous High Temperature Behavior of Near-Equiatomic FeNi Alloys With Dilute Phosphorus Additions
Atomic-Scale Partitioning of Ag and Mg in Ω and T1 Precipitates of Al-Cu(-Li)-Mg-Ag Alloys
Dopant-Driven Grain Boundary Segregation in High Entropy Alloy Nanoparticles
Effect of Ce Content on Solidification Structure in AH36 Steel Ingot: Numerical Simulation and Experimental Study
H-28: Probing Heat Treatment Kinetics to Uncover Sc-Cu Interactions in a Sc-Microalloyed Al-Cu Alloy for Corrosion Design
Oxygen Dynamic Partitioning Endows Superior Strength-Deformability Synergy in Crystalline-Amorphous Nanolaminates
Role of Mo in the Phase Transformation of η-Ni3Ti to Austenite in Fe-Ni-Ti-Mo-Based Maraging Steels
Role of Segregation in Strengthening: Separating Suzuki and Cottrell Effects
Using Orientation to Optimize the Electrically Induced Phase Transformation Conditions in Pure and Doped Zirconia

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