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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Cutting-Edge Characterization and Electrochemical Techniques for Unraveling Corrosion Phenomena
Presentation Title Advanced Mechanical Characterization of Chloride-Induced Stress Corrosion Cracking in Stainless Steel
Author(s) Janelle P. Wharry, Ronit Roy, Lucille V Dentice, Nathan T Gehmlich, Thang Duc Nguyen, Haozheng J Qu, Maria A Okuniewski
On-Site Speaker (Planned) Janelle P. Wharry
Abstract Scope This talk will demonstrate advanced electron microscopy techniques to characterize the elasto-plastic mechanisms of chloride-induced stress corrosion cracking (CISCC) in 304L stainless steel. CISCC, and SCC more generally, has long been characterized using scanning electron microscopy (SEM) to observe features including reaction product layers, pit-to-crack profiles, and crack paths. While these techniques provide significant insight into the nature and morphology of SCC, the roles of elasticity and plasticity (i.e., dislocations) on SCC could only be discerned through time-consuming and localized transmission electron microscopy (TEM). But more recently, high-resolution electron backscatter diffraction (HR-EBSD) enables new insights into the interplay between pitting, cracking, and dislocations. HR-EBSD rapidly maps stress over multiple grains, providing a microscale understanding of dislocation activity previously attainable only through numerous TEM lamellae. Here we apply HR-EBSD to CISCC in 304L stainless steel welds. The attained stress distributions shed new light on the mechanical drivers of CISCC.
Proceedings Inclusion? Planned:
Keywords Iron and Steel, Environmental Effects, Nuclear Materials

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A closer look at passive films upon multi principal element alloys
Advanced Mechanical Characterization of Chloride-Induced Stress Corrosion Cracking in Stainless Steel
Advanced Modeling Techniques for Efficient Discovery of Corrosion Phenomena
Application of Cutting-edge Materials Characterization Techniques to Understanding Stress Corrosion Cracking
Atomic-scale Understanding of Cu Effect on Mechanical, Antibacterial, and Corrosion Properties of Ultrahigh-strength Maraging Stainless Steel
Characterizing the mechanisms controlling localized corrosion of steel in concrete
Combined hydrogen permeation based potentiometry and electrochemical impedance spectroscopy technique to measure cathodic oxygen reduction kinetics at an organic coating/iron interface
Evaluating Passive Film Properties of Fe-Based Metallic Glasses for Enhanced Corrosion Resistance
Evaluation of SS316 Corrosion in a Flowing LiCl-KCl Environment with Real-Time Electrochemical Monitoring
Gathering Actionable Corrosion Data for Light Water Reactors and Molten Salt Reactors
Localized Hydrogen Irradiation of Metals Produced by Focused Ion Beam - Scanning Electron Microscope
Mapping the heterogeneous charge transport during oxidation of metals containing nanoscale metal inclusions with 4DSTEM and APT
Multimodal characterization of material degradation in nuclear environments
Non-Destructive Characterization of Metal-Coating Interface Revealing Corrosion Beneath the Coating
Perspectives on the development of oxidation-resistant alloys for Advanced Ultra-Supercritical power plants
Real-Time Atomic-Scale Imaging of Defect-Driven Oxidation Under Reactive Gases
Revisiting Transpassivity with a new lens: Transpassive corrosion mechanisms in Ni probed with in situ respirometry coupled electrochemical polarization
Scanning Kelvin Probe Techniques for Unraveling Corrosion Phenomena
Uncovering Atomic Scale Corrosion and Oxidation Mechanisms in Materials: Insights from Cryogenic Atom Probe Tomography and Atomic Force Microscopy
Understanding the Influence of Secondary Phase Particles on Localized Corrosion of Al A356 Alloy to Enable an Increased Use of Recycled Al
Whole-surface EBSD mapping for 1:1 correlation of grain structure and corrosion initiation

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