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Meeting MS&T25: Materials Science & Technology
Symposium Engineering Ceramics: Microstructure-Property-Performance Relations and Applications
Presentation Title Small Tests that Make a Big Difference: Correction of the Plastic Size Effect During Micromechanical Testing
Author(s) Alyssa Stubbers, Sajjad Hossain, Christopher Weinberger, Gregory Thompson
On-Site Speaker (Planned) Alyssa Stubbers
Abstract Scope Size effects in micromechanically tested materials arise due to convergence of a material’s plastic zone size and tested specimen size. This makes interpretation of micro-specimen testing difficult, where plasticity characteristics artificially inflate reported fracture toughness values. However, we hypothesize that it is possible to deconvolute plasticity effects from toughness values based on theoretical plastic zone size. Here we describe fabrication techniques of single grain cantilevers in W, Ta2C, and HfC. When used with computational techniques we evaluated distortion effects of plasticity on measured fracture toughness values. Results showed as specimen thickness (B) approaches plastic zone size (ry) there is an increase in reported fracture toughness that can be described by the relationship (0.9ry^2/B^2). From this observation, we proposed an adjustment factor that corrected W, Ta2C, and HfC specimens to agree with calculated KI. Our results facilitate use of micromechanical testing as a quantitative method for materials characterization regardless of scale.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Statistical Model of Microstructural Toughening in Ceramics
Breaking the Charge Neutrality Boundary in Perovskite Using the PyCALPHAD Approach
D-14: Effects of Electrode and Substrate Optimization on Solid Oxide Cell Performance
Design and Sintering of Ceramic-Metal Composites for Extreme Environment Applications
Development of a Li-Corrosion Resistant Coating for Mullite-Cordierite-Based Refractory
Effect of Carbon on the Microstructure and Phase Evolution of High Entropy Dual Phase Ceramics
Effect of SiO2 Content on High-Temperature Phase Transition and Physical Properties in Calcium Aluminate Cement
Fatigue Behavior of Grain Boundaries in High Thermal Conductivity Silicon Nitride Ceramics Evaluated by Microcantilever Bending Test
Finite Element Modeling of Microwave-Assisted Calcination of SOEC Perovskite Precursor Powders
Firing Behavior of 18th Century European Porcelains
Hybrid Microwave Sintering of Electrolytes for SOEC/SOFC Applications
Measurement of Glaze Thermal Expansion via Crazing
Microstructure Development of Electro-Conductive Aluminum Nitride for Sensor Applications
Percolation-Driven Thermal Conductivity Improvement in Pyrolyzed MXene/SiOC Nanocomposites
Reduction Behavior of Mullite/Andalusite-Based Refractories Under Hydrogen Atmosphere and the Effect of Crystalline SiO2 on Mechanical Strength
Small Tests that Make a Big Difference: Correction of the Plastic Size Effect During Micromechanical Testing

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