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Meeting MS&T25: Materials Science & Technology
Symposium Additive Manufacturing of Ceramic-Based Materials: Process Development, Materials, Process Optimization and Applications
Presentation Title Atomic Layer Deposition (ALD) for Nanoscale SiC AM Feedstock Improvement
Author(s) Chris Gump, Guillermo Rojas, Dane Lindblad, Casey Christopher, Tommy Martin
On-Site Speaker (Planned) Chris Gump
Abstract Scope Forge Nano has used ALD to modify SiC AM feedstock surfaces. ALD uses self-limiting surface reactions to deposit nanoscale films onto surfaces with subnanometer precision. Previously coated Ti64 and AlSi10Mg AM feedstocks demonstrated that ALD films increased feedstock oxidation resistance and flowability, and improved mechanical properties printed parts.100 g batches of SiC were coated with 1 – 3 nm of SiO2 in our research fluidized bed reactor. ICP and Leco C and O elemental analysis proved ineffective at characterizing the films, but FIB/STEM imaging and EDS elemental mapping showed uniformly coated particles, with film thickness scaling with the number of ALD cycles performed. The deposition process was scaled to 3 kg batches in our pilot reactor. We expect this material to exhibit improved flowability, densification and mechanical properties in binder jet and other similar AM applications. Further scaling to 100-300 kg will be discussed in various deposition tools.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Additive Manufacturing of Oxide and Non-Oxide Ceramics for Functional and Structural Applications
Advanced Manufacturing and Densification Techniques for Fabricating Ceramic Matrix Composites
Atomic Layer Deposition (ALD) for Nanoscale SiC AM Feedstock Improvement
Colloidal Material Design for Additively Manufacturing Optical Glasses
Development of Aluminium Coating via DC Pulse Electrophoretic Deposition on Inconel 625 Particles for High-Temperature Applications
Development of Direct Ink Write Radially Graded Alumina/Zirconia
Development of Models for Densification and Microstructural Evolution of Ceramic Green Bodies Produced by Direct Ink Writing
Effect of Bimodal Powder on the Densification of a Green Body via Binder Jetting
Effect of Dispersants on the Direct Ink Write Printability of SiC Powder in Phenolic Resin for Sintered SiC
Engineering the Physicochemical Characteristics of Additively Manufactured Ceramics
Expanding Laser Powder Bed Fusion to Functional Ceramics: Bulk Mo₂C Cathodes for Catalysis
Extrusion Manufacturing (Direct Ink Write) of Carbon-Loaded Ultra-High Temperature Ceramic Matrix Composites
Functional Defects in Advanced Ceramics Fabricated by Selective Laser Sintering
Influence of Compositional and Structural Design on the Quasi-Static and Dynamic Performance of Additively Manufactured Silica-Based Ceramics
Metal Elements Doped Negative Poisson's Ratio Based Structural SiOC Polymer-Derived Ceramic to Activate Efficient Pressure and High-Temperature Difunctional Detection Performance
Multi-Material Direct Ink Writing for Ceramic Nuclear Fuel Applications
Multiphysics Modeling of Volumetric Additive Manufacturing with Microwave Beamforming for Ceramic 3D Printing
Photonic Curing of Chemically Bonded Phosphate Ceramics (CBPC) via Flash Lamp Annealing and the Effect of Optical Absorbers on the Reaction Kinetics and Microstructure
Plasma Jet Oxidation of Additively Manufactured Monolithic and High Entropy Ultra High Temperature Ceramic Carbides
Powder Behavior Simulation for Ceramic Additive Manufacturing: Enhancing Process Understanding and Material Performance
Promoting Melting and Solidification of Aluminum Nitride Through Laser Powder Bed Fusion
Tailoring Material Properties of 3D Printed Alumina Through DLP Printing and Firing Parameters
Three-Dimensional Printing of Hierarchically Porous Ceramics for Multifunctional Applications
Towards Microwave Volumetric Additive Manufacturing for Ceramics: Beamforming Experiments
Understanding Slurry Degradation in Digital Light Processing of High Refractive Index Ceramics
Versatile Ceramic Slurry Formulations for Photopolymerization-Based Additive Manufacturing
Viscosity Adjustment Without Binder

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