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Meeting MS&T24: Materials Science & Technology
Symposium Advanced Materials for Harsh Environments
Presentation Title Stabilization Optimization of High Temperature Irradiation Resistant Thermocouples
Author(s) Scott Riley, Brandon King, Kyle Holloway, Allyssa Bateman , Richard Skifton, Brian Jaques
On-Site Speaker (Planned) Scott Riley
Abstract Scope The pursuit of safer, more economic energy production from both existing nuclear reactors and Generation IV reactor designs has pushed the development of in-core instrumentation. The INL has developed high-temperature irradiation-resistant thermocouples (HTIR-TCs) for temperature sensing inside Generation IV nuclear reactors. These thermocouples are composed of phosphorus-doped niobium (Nb-P) and lanthana-doped molybdenum (Mo-LaO) thermoelements, an alumina (Al2O3) insulation, and a niobium sheath. HTIR-TCs require an initial heat treatment exceeding the maximum service temperature to stabilize the generated electromotive force (EMF) signal. Herein, a study was conducted to evaluate multiple stabilizing heat treatments for long term operations: namely, a traditional thermal heat treatment and Joule heating. The traditional method results in a heterogeneous microstructure and takes days to perform, whereas Joule heating can be conducted in less than an hour. The impact of Joule heating on the microstructure, chemical morphology, and electrical properties will be discussed.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Combating Biofouling: Field Testing of a Lubricant-Infused Antifouling Coating in Marine Environments
Conformal Environmental Barrier Coatings On Additive Manufactured Robust Alloys for Mitigation of Oxidation, Erosion, and Corrosion
Development of Corrosion-Resistant High Entropy Alloy for Nuclear Application
Development of High Operating Temperature Latent Thermal Energy Storage System: Material Challenges
Development of Nuclear Reactor Structural Materials with Low Critical Mineral Concentrations
Effect of TiO2 Addition on the Hot Corrosion Behavior of Yttria-Stabilized Zirconia in the Presence of V2O5 for Thermal Barrier Coatings Application
Embedded High-Temperature Sensors: Enhancing Thermoelectrical Performance with Refractory Composites Gradient Layers
Enhancing Sustainability in Tool Repair: Refurbishing H13 Hot Forging Tools Using Laser Directed Energy Deposition
Far-Field Passive Ceramic Sensors for High-Temperature Environments
H-9: Exposure of Aerosol Jet Printed h-BN/Polyimide Nanocomposite Films to Gamma Radiation
High-Temperature Oxidation Behavior of Wrought and Additive Manufactured H282 in Direct-Fired Supercritical CO2 Power Cycle Environments
Hot Corrosion Characteristics of 8YSZ Doped with CSZ and YTiZ in Molten V2O5 for Potential Use in Thermal Barrier Coatings
Hot Corrosion of Mo-Si-B and Its Derivates with Ti or Cr between the 500°C - 900°C Range
How Large Language Models can Discover and Design New Materials?
Incipient Deformation and Fracture of Metals and Ceramics During Dynamic Loading and Ballistic Impact
Increasing the Service Life of Materials Working in Harsh Conditions of Metallurgical Production
Influence of Water Vapor on Hot Corrosion of Nickel-Based Superalloys
Near-Field Passive Wireless Sensor for High-Temperature Metal Corrosion Monitoring
One-Dimensional Wormhole Corrosion in Metals
Pathways to Grain Boundary Engineering in Metal Additive Manufacturing
Preparation of Alitized Coatings Using Functionally Active Charges Operating in Harsh Environments of Coke Production
Refractory Ceramics for Use in Molten Oxide Electrolysis
Stabilization Optimization of High Temperature Irradiation Resistant Thermocouples

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