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Meeting 2027 TMS Annual Meeting & Exhibition
Symposium Spectroscopic Methods and Analysis for Nuclear Energy Related Materials
Presentation Title Determination of High Temperature Mechanical Properties of Nuclear Fuel Using Temperature Resonant Ultrasound Spectroscopy
Author(s) Deana Tsang, Tannor Munroe, Adrien Terricabras, Boris Maiorov, Joshua White
On-Site Speaker (Planned) Deana Tsang
Abstract Scope Resonant Ultrasound Spectroscopy (RUS) is a non-destructive characterization technique for the measurement of bulk elastic properties of materials. The technique relies on the transmittance of an acoustic wave through the sample which activates resonance modes at specific frequencies that are characteristic of the chemistry, crystal structure and density of the material. The spectrum produced is then used to extract the elastic constants. For nuclear fuels, capturing mechanical property information at elevated temperatures is notoriously difficult. This has led to data gaps, particularly for fuels that are challenging to handle due to their pyrophoricity such as UN. Therefore, there exists motivation to develop high temperature thermomechanical characterization tools. Here, we demonstrate the use of RUS to measure Young’s, Bulk and Shear modulus for various nuclear fuels (UO2, doped UO2 and UN) as well as adaptation of the apparatus resulting in temperature-dependent elastic moduli data up to 1000 °C.
Proceedings Inclusion? Planned:
Keywords Nuclear Materials, Mechanical Properties, High-Temperature Materials

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advancing Neutron Scattering Techniques for Nuclear Materials
Application of Synchrotron X-ray Absorption Spectroscopy to Nuclear Materials
Characterizing Nuclear Energy Related Materials with Laser Ablation Laser Ionization (LALI) Mass Spectrometry
Chemical bonding in UO3 polymorphs: a QTAIM–Hessian-matrix perspective on short U–O and oxo bonds
Determination of High Temperature Mechanical Properties of Nuclear Fuel Using Temperature Resonant Ultrasound Spectroscopy
High temperature Raman spectroscopy of in-situ annealing of ion irradiated SiC and residual stresses in SiC/SiC composites
In-situ Raman Spectrometry of Passive Surface Layers on Stainless Steel
In-Situ UV–Vis Quantification of Chlorobasicity in Binary Molten Chlorides: A Spectroscopic Framework for Molten Salt Reactor Chemistry
Irradiation-damage Response of Stable Grain-boundary-decorated Nanocrystalline Multi-principal-element Alloy
Linking Atomic Structure to Engineering Performance in Refractory Materials for Fusion and Fission
Multimodal chemical imaging and microanalysis of intermetallic materials
NMR Spectroscopy of Zirconium Carbides after High-Temperature Hydrogen Exposure
Nuclear Materials Research using the Activated Materials Laboratory and the Advanced Photon Source
One dislocation, one pore at a time: Probing radiation damage in nuclear materials
Potential of atom probe tomography for mapping hydrogen isotopes in nuclear materials
Raman Spectroscopy of Lanthanides in LiCl-KCl Eutectic for Nuclear Energy Systems
Real-Time Spectroscopic Characterization of Molten Salt Systems Using Electrochemical–LIBS Data Fusion and Probabilistic Neural Networks
Surface-Sensitive X-ray Absorption Spectroscopy for Investigating Corrosion Mechanisms in Actinide Metals
Synchrotron-based high-{energy/temperature/strain/modality} characterization resources for nuclear materials research at NSLS-II
Three-Dimensional Characterization of Crack and Inclusion Networks in a Service-Exposed Baffle Former Bolt Using High-Energy X-Ray Microscopy
Understanding Temperature in Extreme Conditions

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