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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Material Responses Investigated Through Novel In-Situ Experiments and Modeling
Presentation Title In-Situ Ultrasonic Mapping of Phase Transformation Behavior in NiTi Shape Memory Alloys
Author(s) Olivia J. Cook, Andrea P. Argüelles
On-Site Speaker (Planned) Olivia J. Cook
Abstract Scope Current characterization methods for martensitic phase transformations in shape memory alloys such as differential scanning calorimetry are unable to capture spatial variations within larger components. While ultrasonic wave speed measurements have detected these transformations, existing approaches lack the spatial resolution and necessary analytical framework to quantitatively assess transformation kinetics across bulk specimens. This study introduces spatially-resolved ultrasonic mapping of thermal phase transformations in NiTi specimens using a temperature-controlled immersion fluid. The methodology provides real-time spatial visualization of martensitic transformation progression between parent and product phases, revealing heterogeneous behavior in wrought specimens. Analytical modeling grounded on ultrasonic scattering in polycrystalline microstructures enables quantitative interpretation of the spatially-varying data and associated transformation kinetics. This integrated approach addresses critical gaps in process-structure-property relationships by determining whether small-scale specimen behavior represents bulk material response. Findings could impact shape memory alloy manufacturing and fabrication of heterogeneous components with tailored properties.
Proceedings Inclusion? Planned:
Keywords Characterization, Phase Transformations, Other

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Analysis of the Plastic Deformation Mechanisms of Extruded Pure Zn Through In-Situ SEM/EBSD
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Elucidating the Response of Solute Clusters and Precipitates to Tensile Loading in Recycled Wrought Al-Mg-Si Alloy Using In-Situ Small-Angle Scattering
Experimental–Numerical Micromechanical Analysis of Silicon Micro-Scratching
Fracture Toughness of (CrMoTaVW)C
G-25: Quantitative Characterization of Local Deformation in Steels Exhibiting Macroscopic Inhomogeneous Deformation Bands
Grain-Scale Plastic Deformation Transmission Prediction in Ti-7Al During Creep Using High-Energy Diffraction Microscopy and Graph Neural Networks
How Does Irradiation, Microstructure and Temperature Affect Deformation in Ferritic-Martensitic Steels
Imaging 3D Polarization Dynamics via Deep Learning 4D-STEM
In-Situ Experiments and Simulation of Damping in Micro/Nano Pillar Arrays
In-Situ TEM Analysis of Microstructural Impact on Filament Growth in All Solid-State Sodium Batteries
In-Situ Ultrasonic Mapping of Phase Transformation Behavior in NiTi Shape Memory Alloys
In Situ Synchrotron Thermo-Mechanical Testing With Rotational and Axial Motion Systems IV (RAMSIV)
Influence of Microstructural Heterogeneities on the Plastic Response of Polycrystalline Wire-Arc Additive Manufactured Ni-Al-Bronze
Investigating Grain-Scale Cyclic Strain Accumulation and Damage Localization Under Non-Proportional Axial-Torsional Loading Through In-Situ HEDM and Crystal Plasticity Modeling
Investigating Subgrain Growth During Early-Stage Recrystallization in High-Purity Aluminum With In-Situ EBSD
Mapping Cracks and Their Strain Fields in Microsamples by Complementary In Situ Experiments
Materials Responses During Laser Additive Manufacturing Revealed by X-Rays
Orientation and Temperature Dependence of Deformation Mechanisms in Tantalum: Insights From Micropillar Compression Tests
Plastic Strain Localization at Twin Boundaries in Nickel Under Cyclic Loading: A Three-Dimensional Discrete Dislocation Dynamics Study
Quantitative Imaging Methods for Deciphering Stability in Nanocrystalline Metals
Slip Band Evolution and Localized Deformation in Polycrystals: A Coupled XFEM and CPFEM Study
Thermal Conductivity Measurement of a Thin Layer of the Single Crystals of β Phase Lead Oxide Using Time Domain Thermoreflectance (TDTR) Technique
Tracking Cerium Oxidation Pathways via In-Situ Atom Probe Tomography
Using High-Energy Diffraction Microscopy and Tomography to Assess Phase-Field Fracture Models for Brittle Fracture

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