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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Recent Advances in Electron Back-Scattered Diffraction and Related Techniques
Presentation Title HREBSD Through Spherical Harmonic Transform Indexing for Characterizing Subgrains
Author(s) Thomas J. Bennett, Eric M. Taleff
On-Site Speaker (Planned) Thomas J. Bennett
Abstract Scope Subgrains produced in metals during deformation under five-power creep at elevated temperatures are distinguished by low-angle boundaries with misorientations as small as a few tenths of a degree. High-resolution electron backscatter diffraction (HREBSD) provides sufficient angular resolution to measure subgrain boundaries and enables characterization of large samples of subgrains not readily accessible using other techniques. We demonstrate that spherical harmonic transform (SHT) indexing can produce HREBSD orientation data sufficient for this purpose and provides distinct advantages over the more common cross-correlation methods. HREBSD data are presented for large populations of subgrains in an interstitial-free steel that was deformed at 850 °C. Changes in the distributions of subgrain size and boundary misorientation with increasing plastic strain, as measured from HREBSD data, provide important insights into microstructure evolution during high-temperature deformation. SNL is managed and operated by NTESS under DOE NNSA contract DE-NA0003525.
Proceedings Inclusion? Planned:
Keywords Characterization, Mechanical Properties, Iron and Steel

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Applications of Electron Backscatter Diffraction to Aerospace Materials
Combining Low Voltage EBSD with Spherical Indexing for Optimal Results
Deep Learning Application for Simultaneous Kikuchi and Spot Pattern Acquisition and Indexing SEM
EBSD to Characterize Plasticity at the Sub-Grain Level: A Complementary Response to HR-DIC
Energy-Resolved Measurement of Backscattered Electrons in EBSD Using a Monolithic Direct Electron Detector
Experimental and Simulation Insights Into Unintended Electron Beam-Induced Heating in SEM Experiments
HREBSD Through Spherical Harmonic Transform Indexing for Characterizing Subgrains
Investigations of Dental Zirconia Deformation Mechanisms Using EBSD Spherical Indexing
Nanoscale Quantification of Twinning Shear and Martensite Transformation Strain by In Situ TKD-DIC Tensile Testing
Near-Axis TKD for Improving Spatial Resolution
On the Use of High Angular Resolution Orientation Similarity Maps for the Study of Dislocation Walls in Metallic Microstructures
Orientation-Adaptive Virtual Imaging of Defects Using EBSD
Phase Detection in Martensitic Steels by EBSD at Lower Accelerating Voltages
Rapid and Correlative EBSD Characterisation of HP-Micro Alloy and its Variants
Resolving Overlapping EBSD Patterns Using Iterative Dynamic Template Matching
Sub-Grain Detection in EBSD Datasets Using Clustering Algorithms in Machine Learning
Towards Absolute Non-Simulation-Based HR-EBSD on Single Experimental Patterns, by Means of Excess-Deficiency Correction
Uncertainty in High-Angular-Precision 3D-EBSD Orientation Measurements Using Spherical Harmonic Indexing and Global Pattern Center Optimization on Deformed and Undeformed Samples
Using Particle Swarm Optimization for Finding the Pattern Center in EBSD
Using Spherical Indexing to Identify Polytypes, Stacking Irregularities and Domain Structures in Late Transition Metal Stannides

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