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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Neutron Scattering for Engineering Materials
Presentation Title Development and Commissioning of an In Situ ³He Polarizer for Polarized Neutron Diffraction Studies at VULCAN
Author(s) Sichao Fu, Chenyang Jiang, Dunji Yu, Yan Chen, Lowell Crow, Ke An
On-Site Speaker (Planned) Sichao Fu
Abstract Scope An in situ ³He polarizer has been developed for the engineering materials diffractometer VULCAN at the Spallation Neutron Source, Oak Ridge National Laboratory, to enable concurrent investigations of deformation and magnetic dynamics under combined external fields. The polarizer employs spin-exchange optical pumping (SEOP) to polarize ³He gas in situ. The polarization level is monitored using free induction decay (FID) nuclear magnetic resonance (NMR), and spin direction can be flipped via adiabatic fast passage (AFP) NMR. The system is compatible with various sample environments—including load frames, furnaces, and magnetic fields—allowing studies under mechanical, thermal, and magnetic stimuli, either individually or in combination. A commissioning experiment on a NiMnGa magnetic shape memory alloy, using a mini load frame and magnet yoke, demonstrated the polarizer’s capability. Polarized neutron diffraction measurements successfully captured magnetic domain evolution correlated with deformation-induced twinning.
Proceedings Inclusion? Planned:

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Current Residual Stress Neutron Diffractometer at the High Flux Isotope Reactor (HIDRA) and Proposed Upcoming Upgrades
Development and Commissioning of an In Situ ³He Polarizer for Polarized Neutron Diffraction Studies at VULCAN
Effects of CO2 reactions on rock microstructure
Extinction-based diffraction analysis of phase transformation and recovery in β-Zr and β-Ti alloys
In situ neutron diffraction and Bragg-edge imaging for residual stress mapping in laser powder bed fusion
Neutron Imaging at the MIT Reactor: Capabilities and Applications in Batteries and Metal Hydrides
Neutron Imaging at the Multimodal Advanced Radiography Station
Neutron techniques as complementary tools for materials characterization - an industrial prospective
Small Angle Neutron Scattering As a Tool For Engineering Materials Microstructure Characterization
Understanding and Controlling Residual Stress Evolution in Welded Large-Scale Stainless Steel Structures
Understanding Processing, Structure and Behavior of Engineering Materials at the Engineering Neutron Diffractometer VULCAN

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