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Meeting MS&T25: Materials Science & Technology
Symposium Engineering Ceramics: Microstructure-Property-Performance Relations and Applications
Presentation Title Fatigue Behavior of Grain Boundaries in High Thermal Conductivity Silicon Nitride Ceramics Evaluated by Microcantilever Bending Test
Author(s) Junichi Tatami, Komaki Matsuura, Motoyuki Iijima, Takuma Takahashi, Tatsuki Ohji, Hiromi Nakano
On-Site Speaker (Planned) Junichi Tatami
Abstract Scope In this study, we aimed to clarify the fatigue behavior of grain boundaries in high thermal conductivity silicon nitride ceramics by microcantilever bending tests. First, a spherical indenter was repeatedly pressed into a mirror-polished surface to simulate the stress state in a copper-plated substrate. The strength of the grain boundary on the surface was measured by a microcantilever bending test. The results showed that the grain boundary strength decreased with repeated application of stress. The grain boundary strength decreased with repeated stress application to the microcantilever specimen, which was prepared with the grain boundary at the root, suggesting that the accumulation of such dislocations near the surface was the source of stress concentration that reduced the grain boundary strength. The TEM observation showed many dislocations in the near-surface region.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Statistical Model of Microstructural Toughening in Ceramics
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Development of a Li-Corrosion Resistant Coating for Mullite-Cordierite-Based Refractory
Effect of Carbon on the Microstructure and Phase Evolution of High Entropy Dual Phase Ceramics
Effect of SiO2 Content on High-Temperature Phase Transition and Physical Properties in Calcium Aluminate Cement
Fatigue Behavior of Grain Boundaries in High Thermal Conductivity Silicon Nitride Ceramics Evaluated by Microcantilever Bending Test
Finite Element Modeling of Microwave-Assisted Calcination of SOEC Perovskite Precursor Powders
Firing Behavior of 18th Century European Porcelains
Hybrid Microwave Sintering of Electrolytes for SOEC/SOFC Applications
Measurement of Glaze Thermal Expansion via Crazing
Microstructure Development of Electro-Conductive Aluminum Nitride for Sensor Applications
Percolation-Driven Thermal Conductivity Improvement in Pyrolyzed MXene/SiOC Nanocomposites
Reduction Behavior of Mullite/Andalusite-Based Refractories Under Hydrogen Atmosphere and the Effect of Crystalline SiO2 on Mechanical Strength
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