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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Vacancy Engineering in Metals and Alloys
Presentation Title Quantifying Irradiation Damage with 4D-STEM
Author(s) Andrew M. Minor, Dongye Liu, Sean Mills
On-Site Speaker (Planned) Andrew M. Minor
Abstract Scope Nanoscale irradiation damage in materials such as vacancies, bubbles, voids, black spot damage and small radiation loops can be notoriously difficult to directly image, and even more difficult to accurately quantify. Often the strain fields or structures themselves overlap, even in thin foils used for electron microscopy. This talk will describe our recent work using 4D-STEM (nanobeam electron diffraction imaging) to quantify irradiation defects. We will discuss the pros and cons of 4D-STEM in comparison to well-established electron microscopy techniques (HRSTEM, BF/DF) for imaging and quantifying nanoscale defects in irradiated materials. Examples will be provided from irradiated pure metals such as Au, Fe, and Cr, as well as the Ni-Cr alloy system where irradiation is coupled with molten salt corrosion.
Proceedings Inclusion? Planned:
Keywords Characterization, Nuclear Materials, Environmental Effects

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A combined physics-based and data-driven prediction of vacancy formation energies in refractory non-dilute random alloys
Assessing the Mechanical Properties of Iron Aluminides: Strength and Brittle-to-Ductile Transition
Assessing Vacancy-Solute Clustering and Void Nucleation in Magnesium Alloys Via Transition Interface Sampling
Design of radiation-resistant dilute alloys using synergistic solutes to trap vacancies
Direct Simulation of Vacancy Transport During Creep Deformation in Coupled Extreme Environments
Dynamic microstructure stabilization via self-organization on grain boundaries in dilute nanocrystalline alloys
Effect of Sn microalloying and vacancies on diffusion of Zr in Aluminum
Enhancing radiation tolerance via defect engineering
Grain boundary migration during irradiation and oxidation of alloys
High Strength and Ductile, Single-Phase, Refractory Multi-Principle-Element Alloys (RMPEAs) by Theory-Guided Tailoring: Effects of Chemical Short-Range Order, Vacancies, and Hydrogen
How Alloying Elements Shape Vacancy-Induced Solute Clustering in Binary Magnesium Alloys
Hydrogen's Influence on Vacancy Diffusion in Metals: Inhibitor or Catalyst?
Influence of thermo-mechanical processing on ordering kinetics in 18 karat red gold alloy
Insights of Nano-Void Nucleation and Solute Aggregation in Magnesium Alloys Using Transition Interface Sampling
Investigating nanocavity formation kinetics in irradiated materials through elemental segregation
Irradiation-Enhanced Transport in Model Oxides: Insights from Isotopic Tracers and Atom Probe Tomography
Modeling the Potential Energy Landscape of Vacancies in Nickel Superalloys Using Atomistic Simulations and Machine Learning
Modelling the role of impurity trapping in excess vacancy evolution and its influence on age hardening behaviors in multicomponent aluminium alloys
Multiscale Modeling of Vacancy Trapping and Clustering Kinetics in Multicomponent Alloys
Nanoscale vacancy mapping in metals by four-dimensional scanning transmission electron microscopy (4D-STEM)
Positron annihilation spectroscopy in Mg and Mg-alloys
Quantifying Irradiation Damage with 4D-STEM
Stabilizing solute clusters in low-alloy steels: Effects of excess vacancies and impurity interactions
Time–temperature superposition for the spall strength of light metals with nonequilibrium vacancy concentrations
Vacancy-Driven Irradiation-Induced Amorphization and Crystallization in Nanostructured Materials
Vacancy-driven phase stability phenomena in ion irradiated alloys
Vacancy-Mediated Diffusion in Complex Materials Quantified with Machine Learning
Vacancy and self-interstitial radiation defects in fusion power plant materials and their effect on reactor operation.
Vacancy Evolution in Structural Alloys and High-Entropy Ceramics under Extreme Irradiation Conditions

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