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Meeting 2026 TMS Annual Meeting & Exhibition
Symposium Recent Advances in Electron Back-Scattered Diffraction and Related Techniques
Presentation Title Near-Axis TKD for Improving Spatial Resolution
Author(s) Michael Hjelmstad, Kim Larsen, Mark Coleman, Angus Bewick
On-Site Speaker (Planned) Michael Hjelmstad
Abstract Scope Transmission Kikuchi Diffraction (TKD) was a breakthrough technique that improved the spatial resolution of microstructural mapping (EBSD in SEM) to roughly 10nm. Originally, an off-axis geometry that used traditional EBSD hardware was employed. Although it was an easier approach, it required high beam currents to achieve good signal. An on-axis technique was later developed that produced less distortion in patterns with good signal but required a means of removing the transmitted electron beam from the Kikuchi patterns. To take the positive of both setups, we have developed “Near-Axis TKD (NA-TKD).” The NA-TKD setup can be used at short working distance with zero sample tilt and a lower beam current, all variables that will improve spatial resolution. The detector can be tilted to optimize sample-to-screen distance and incorporates brightfield and darkfield STEM imaging. The talk will explore optimization of setup parameters to achieve sub-10nm spatial resolution.
Proceedings Inclusion? Planned:
Keywords Characterization, Other,

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Applications of Electron Backscatter Diffraction to Aerospace Materials
Combining Low Voltage EBSD with Spherical Indexing for Optimal Results
Deep Learning Application for Simultaneous Kikuchi and Spot Pattern Acquisition and Indexing SEM
EBSD to Characterize Plasticity at the Sub-Grain Level: A Complementary Response to HR-DIC
Energy-Resolved Measurement of Backscattered Electrons in EBSD Using a Monolithic Direct Electron Detector
Experimental and Simulation Insights Into Unintended Electron Beam-Induced Heating in SEM Experiments
HREBSD Through Spherical Harmonic Transform Indexing for Characterizing Subgrains
Investigations of Dental Zirconia Deformation Mechanisms Using EBSD Spherical Indexing
Nanoscale Quantification of Twinning Shear and Martensite Transformation Strain by In Situ TKD-DIC Tensile Testing
Near-Axis TKD for Improving Spatial Resolution
On the Use of High Angular Resolution Orientation Similarity Maps for the Study of Dislocation Walls in Metallic Microstructures
Orientation-Adaptive Virtual Imaging of Defects Using EBSD
Phase Detection in Martensitic Steels by EBSD at Lower Accelerating Voltages
Rapid and Correlative EBSD Characterisation of HP-Micro Alloy and its Variants
Resolving Overlapping EBSD Patterns Using Iterative Dynamic Template Matching
Sub-Grain Detection in EBSD Datasets Using Clustering Algorithms in Machine Learning
Towards Absolute Non-Simulation-Based HR-EBSD on Single Experimental Patterns, by Means of Excess-Deficiency Correction
Uncertainty in High-Angular-Precision 3D-EBSD Orientation Measurements Using Spherical Harmonic Indexing and Global Pattern Center Optimization on Deformed and Undeformed Samples
Using Particle Swarm Optimization for Finding the Pattern Center in EBSD
Using Spherical Indexing to Identify Polytypes, Stacking Irregularities and Domain Structures in Late Transition Metal Stannides

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