About this Abstract |
| Meeting |
2024 TMS Annual Meeting & Exhibition
|
| Symposium
|
Characterization of Minerals, Metals and Materials 2024: Process-Structure-Property Relations and New Technologies
|
| Presentation Title |
Synthesis and Electrical Characterization of Ba1-x/2Ti1-xNbxO3 Ceramics |
| Author(s) |
F.R. Barrientos-Hernández, Miguel Pérez Labra, Martín Reyes Pérez, José Agustín Palmas León, Edgar Cardoso Legorreta, Juan Pablo Hernández Lara, Edgar Ramírez Martínez, Iván Alonso Lira Hernández, Ramiro Escudero García |
| On-Site Speaker (Planned) |
F.R. Barrientos-Hernández |
| Abstract Scope |
The synthesis and electrical characterization of compositions based on Nb5+ doped BaTiO3 was carried out using the Ba1-x/2Ti1-xNbxO3 mechanism, and x= 0.001, 0.003, 0.005, 0.04, 0.08, 0.20 and 0.25 de Nb5+ by the solid-state reaction (SSR). All compositions were ground in PET containers with a capacity of 0.5 liter with zirconia balls as a milling means for 5 hours and acetone as a control agent. The resulting powders were carried out a complete decarbonation at 1000 ºC for 5 hours, followed by a double sintering temperature from 1100 ºC to 1500 ºC. In SEM micrographs corresponding to x = 0.001 and 0.003 grooves observed due to of the grain boundaries growth. In the diffractogram x= 0.005 a doublet can be seen at ≈45º, for x= 0.04 the double peak is observed at ≈55º, which indicates the tetragonal distortion of the cubic cell. |
| Proceedings Inclusion? |
Planned: |
| Keywords |
Characterization, Ceramics, Electronic Materials |