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Meeting 2027 TMS Annual Meeting & Exhibition
Symposium Spectroscopic Methods and Analysis for Nuclear Energy Related Materials
Presentation Title Linking Atomic Structure to Engineering Performance in Refractory Materials for Fusion and Fission
Author(s) David Sprouster, Jiao Li, Kent Christian, Leyla Yanmaz, Elyce Milligan, Eden Estes-Lumpkin, Jarrett Moon, Takaaki Koyanagi, Weicheng Zhong, Yutai Katoh, Steve Zinkle, Lance Snead, Daniel Winklehner, Nick Brown
On-Site Speaker (Planned) David Sprouster
Abstract Scope Advanced fusion and fission energy systems require refractory materials capable of maintaining structural integrity under extreme combinations of neutron irradiation, energetic particles, and high temperatures. This presentation highlights recent advances in understanding the degradation and performance of tungsten and tungsten-based ultra-high-temperature ceramics (UHTCs) through complementary structural, thermophysical, and mechanical characterization. Synchrotron X-ray diffraction, X-ray absorption spectroscopy, and laboratory-based techniques are used to quantify irradiation- and thermally induced changes in crystal structure, phase stability, nanoprecipitate evolution, thermal conductivity, fracture resistance, and microstructural stability. Results from neutron-irradiated tungsten alloys are compared with emerging W-based UHTCs and advanced carbides developed for both fusion plasma-facing components and targets for accelerator-driven systems. Together, these studies identify the atomic- and microstructural mechanisms governing radiation tolerance and property evolution while demonstrating how integrated, multiscale characterization can accelerate the design, optimization, and qualification of next-generation refractory materials for extreme nuclear environments.
Proceedings Inclusion? Planned:
Keywords High-Temperature Materials, Characterization, Nuclear Materials

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advancing Neutron Scattering Techniques for Nuclear Materials
Application of Synchrotron X-ray Absorption Spectroscopy to Nuclear Materials
Characterizing Nuclear Energy Related Materials with Laser Ablation Laser Ionization (LALI) Mass Spectrometry
Chemical bonding in UO3 polymorphs: a QTAIM–Hessian-matrix perspective on short U–O and oxo bonds
Determination of High Temperature Mechanical Properties of Nuclear Fuel Using Temperature Resonant Ultrasound Spectroscopy
High temperature Raman spectroscopy of in-situ annealing of ion irradiated SiC and residual stresses in SiC/SiC composites
In-situ Raman Spectrometry of Passive Surface Layers on Stainless Steel
In-Situ UV–Vis Quantification of Chlorobasicity in Binary Molten Chlorides: A Spectroscopic Framework for Molten Salt Reactor Chemistry
Irradiation-damage Response of Stable Grain-boundary-decorated Nanocrystalline Multi-principal-element Alloy
Linking Atomic Structure to Engineering Performance in Refractory Materials for Fusion and Fission
Multimodal chemical imaging and microanalysis of intermetallic materials
NMR Spectroscopy of Zirconium Carbides after High-Temperature Hydrogen Exposure
Nuclear Materials Research using the Activated Materials Laboratory and the Advanced Photon Source
One dislocation, one pore at a time: Probing radiation damage in nuclear materials
Potential of atom probe tomography for mapping hydrogen isotopes in nuclear materials
Raman Spectroscopy of Lanthanides in LiCl-KCl Eutectic for Nuclear Energy Systems
Real-Time Spectroscopic Characterization of Molten Salt Systems Using Electrochemical–LIBS Data Fusion and Probabilistic Neural Networks
Surface-Sensitive X-ray Absorption Spectroscopy for Investigating Corrosion Mechanisms in Actinide Metals
Synchrotron-based high-{energy/temperature/strain/modality} characterization resources for nuclear materials research at NSLS-II
Three-Dimensional Characterization of Crack and Inclusion Networks in a Service-Exposed Baffle Former Bolt Using High-Energy X-Ray Microscopy
Understanding Temperature in Extreme Conditions

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