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Meeting Materials Science & Technology 2012
Symposium Raymond W. Buckman, Jr. Memorial Symposium for Refractory Metals and Alloys
Presentation Title Post-Irradiation Fracture Toughness of Unalloyed Molybdenum, ODS Molybdenum, and TZM Molybdenum Following Irradiation at 244°C to 507°C
Author(s) Brian Vern Cockeram, L. L. Snead, Thak Sang Byun, J. L. Hollenbeck
On-Site Speaker (Planned) Brian Vern Cockeram
Abstract Scope Commercially available unalloyed molybdenum (Low Carbon Arc Cast (LCAC)), Oxide Dispersion Strengthened (ODS) molybdenum, and TZM molybdenum were neutron irradiated at temperatures of nominally 244°C, 407°C, and 507°C to neutron fluences between 1.0 to 4.6 X 1025 n/m2 (E>0.1 MeV). Post-irradiation fracture toughness testing was performed. All alloys exhibited a Ductile to Brittle Transition Temperature (DBTT) that was defined to occur at 30 ± 4 MPa-m1/2. The highest post-irradiated fracture toughness values (26-107 MPa-m1/2) and lowest DBTT (100-150°C) was observed for ODS molybdenum in the L-T orientation. The finer grain size for ODS molybdenum results in fine laminates that improve the ductile laminate toughening. The results for ODS molybdenum are anisotropic with lower post-irradiated toughness values (20-30 MPa-m1/2) and DBTT (450-600°C) in the T-L orientation. The results for T-L ODS molybdenum are consistent with those for LCAC molybdenum (21-71 MPa-m1/2 and 450-800°C DBTT). The fracture toughness values measured for LCAC and T-L ODS molybdenum at temperatures below the DBTT were determined to be 8-18 MPa-m1/2. Lower fracture toughness values were measured for TZM molybdenum that are attributed to the large carbide precipitates serving as preferential fracture initiation sites. The role of microstructure and grain size on post-irradiated fracture toughness was evaluated by comparing the results for LCAC molybdenum and ODS molybdenum.
Proceedings Inclusion? Definite: A CD-only volume

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Review of Rhenium Processing Technologies
Application of Refractory Materials as Friction Stir Welding Tools
Case Studies in Structure-Property Relationships of High Temperature Materials
Characterization of Microstructural Evolution in Refractory Metals from Deformation and Thermal Processing
Characterizing Dislocation Substructure in Large Grain Niobium for Accelerator Cavities
Comparison of Processing on the Mechanical and Microstructure of Powder Metallurgy Molybdenum 41% and 47.5% Rhenium
Crystal Plasticity Finite Element Modeling of Deformation of Single Crystal Niobium
Current and Developmental Production Methods of W and WC Based Powders
Discussion of High-Temperature Vacuum Creep for Selected Refractory Alloys
Exploring Possibilities of MoRe in Medical Devices
High Strain Rate Effects on Fracture of Niobium Alloy C-103
Manufacturing Processes and Properties of Tungsten-25%Rhenium with and without Hafnium Carbide for Friction Stir Welding Tooling
Mechanical and Physical Metallurgy of High Purity Niobium used for Superconducting Radio Frequency Cavities for Particle Accelerators
Microalloying of Mo-Si Alloys as a Key for Developing Ductile Ultrahigh Temperature Mo-Borosilicide Alloys
Microstructure Development of Ultra-high Temperature Mo-Nb-Si-B Alloys
Molybdenum and Mo Alloys: Processing, Properties, Structure and Applications
Molybdenum in Photovoltaic Technology
Overview of Tantalum Products and Recent Advances in Thin Film and Chemical Processing Applications
Overview of the Refractory Metal Production Capabilities of Plansee USA's Franklin, MA Facility
Post-Irradiation Fracture Toughness of Unalloyed Molybdenum, ODS Molybdenum, and TZM Molybdenum Following Irradiation at 244°C to 507°C
Precipitation Strengthening in Refractory Cr-Ni-Al-Ti Alloys
Refractory Metal Powders for Powder Injection Molding
Selective Doping of Molybdenum and Tungsten
Speaking on Raymond W. Buckman
Speaking on Raymond W. Buckman
Speaking on Raymond W. Buckman
Speaking on Raymond W. Buckman
Speaking on Raymond W. Buckman
Strategies and Test Methods for Evaluating Materials at High Temperatures
The Many Applications of Refractory Metals
The Work Hardening Behavior of Commercial-Purity Rhenium Sheet Compared to Stainless Steel, Brass, and Aluminum
Thermodynamic Modeling of the Mo-Hf-C System and Simulation of Precipitate Evolution in Mo-2Hf-0.2C Alloy

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