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Meeting 2018 TMS Annual Meeting & Exhibition
Symposium Materials and Fuels for the Current and Advanced Nuclear Reactors VII
Presentation Title Corrosion of SiC with Cr, CrN, and TiN Coatings in High Temperature Water
Author(s) Stephen S. Raiman, Peter Doyle, Caen Ang, Kurt A Terrani
On-Site Speaker (Planned) Stephen S. Raiman
Abstract Scope SiC/SiC ceramic matrix composite (CMC) materials are an attractive accident tolerant fuel (ATF) cladding candidate. However, the high dissolution rate of SiC/SiC CMCs in light water reactor (LWR) coolant indicates a need for environmental barrier coatings. For this study, candidate coatings were applied to SiC substrates, and exposed for up to 600h in high temperature water (288-320°C) with added hydrogen or oxygen to mimic LWR conditions. Samples were weighed for mass change, and examined with light microscopy, electron microscopy and Raman spectroscopy. Samples coated with Cr and CrN experienced less mass loss compared to uncoated SiC. TiN coated samples gained mass due to oxide formation, and exhibited the greatest mass gain in BWR normal water chemistry. This work discusses how these findings affect the suitability of the coatings for use in ATF. This work was funded by U.S. Department of Energy’s Office of Nuclear Energy, Advanced Fuel Campaign.
Proceedings Inclusion? Planned: Supplemental Proceedings volume


3D Characterization of High Fluence Irradiated UZr and UMo Fuels
A New Physically Based, Quantitatively Predictive Low Flux-high Fluence Model of RPV Embrittlement
A Study on the High Energy Ball Milling and Spark Plasma Sintering of Fe-Cr Based Alloys
A Unified Model for Irradiation Creep and Stress-free Growth in Zirconium Alloys
Additive Stainless Steel for Nuclear: From Material Aspects to Quality Part
Advanced Characterization of Irradiated UO2 Fuel
Advanced Manufacturing of HT9 Steel for Extreme Environments
Atom Probe Examinations of Zircaloy Irradiated at 358-410C
Atom Probe Tomography Study of Microstructural Evolution of Cast Duplex Stainless Steels after 10,000 Hour Thermal Aging
Characterization of Intragranular Creep Deformation in Uranium Dioxide Using Electron Backscatter Diffraction and Electron Channeling Contrast Imaging
Characterization of the Microstructure and Grain Boundary Character of 14-YWT Nanostructured Ferritic Alloys Following Different Deformation Processing Paths
Characterization of U-Zr-RE Metallic Fuel Fabricated by Injection Casting
Characterizing and Modelling Precipitation in Zirconium Alloys
Chemical and Microstructural Analysis of Irradiated Mixed Oxide Fuels
Chemical Compatibility of Refractory Carbides with Hydrogen at Very High Temperatures Relevant for Nuclear Thermal Propulsion Applications
Comprehensive Characterization of Irradiation Defects in Ferric Nuclear Alloy via STEM-based Microscopy
Corrosion Assessment of an Alloy/Oxide Composite Using Electrochemical Techniques
Corrosion of SiC with Cr, CrN, and TiN Coatings in High Temperature Water
Creep Related Microstructural Evolution of Alloy 617-based ODS Alloy
Development of an Alternative Manufacturing Process for U3Si2 Fuel by a Novel Additive Manufacturing Process
Development of Laves and B2 Manipulated Advanced Ferritic Alloys
Dual Ion Beam Irradiation of Commercial-grade Austenitic Alloys Relevant to LWR Core Components at High Dose
Effect of C and Si Impurities in U10Mo Alloy: Discovery of New Quaternary Si-rich Phase and its Influence on Transformation Kinetics
Effect of Cold Working on the Corrosion and Carburization Behavior of Alloy 800HT in High Temperature CO2 Environment
Effect of Grain Elastic Anisotropy on Stress Intensification at Intergranular Stress Corrosion Cracking Iinitiation Sites in Austenitic Stainless Steels and Nickel-based Alloys in Light Water Reactor Environment
Effect of Neutron Irradiation on the Mechanical Properties and Microstructure of Friction Stir Processed ODS Alloys
Effects of Proton Irradiation on Microstructure in Additively Manufactured 316L Stainless Steel Made by Laser Powder Bed Fusion
Electron Microscopy Analysis of TRISO Fuel Particles with Failed SiC Layers from the AGR-2 Irradiation
Examining the Effects of Neutron Irradiation on Zirconium-alloy Oxide Film Microstructure Using Focused Ion Beam Techniques
Experimental Studies on Microstructure and Mechanical Properties of High Burnup Urania
F-14: Asymptotic Expansion Homogenization of the Stiffness Tensor and Thermal Conductivity of a 2D Exemplar-guided Digital Reconstruction of an Al3Hf-Al Microstructure with Comparison to Experiment
F-15: Characterization of Stress and Microstructure of Zr-4 alloy Processed by Pulsed Laser
F-18: Experimentally Determined Properties of U-Pu-Zr Alloys: What Do We Know and How Well?
Fabrication of Lumped Gd2O3 Inserted Oxide Pellets for Burnable Absorber Fuel
Fabrication of ODS FeCrAl Tube for Accident Tolerant Fuel Cladding Applications
Fabrication of PyC/SiC Diffusion Couples Using Fluidized Bed CVD Techniques for Radiation Enhanced Diffusion Testing
Grain Boundary Engineering for Improved Resistance to Corrosion and Stress Corrosion Cracking Resistance of Nuclear Alloys
High-temperature Mechanical Properties of Zirconium Hydrides Studied with Nanoindentation
High Temperature Strength Characterization of Alloy 709
Impact of Low Dose Ion Irradiation on Raman Spectra and Thermal Conductivity in 3C-SiC
Implementation and Validation of a Physically-based Fuel Cladding Oxidation Model in BISON Nuclear Fuel Performance Code
Improvements and Applications of the FAST Fuel Model to Thorium-based and Mixed Oxide Fuels
In-situ Characterization of Dispersoid Evolution during Annealing of ODS FeCrAl Mechanical Alloyed Powders
In-situ Elevated Temperature Micro-cantilever Testing of UO2
In-situ TEM Observation and MD Simulation of the Radiation Defects near Carbon Nanotube in Aluminum
In-situ Testing of Fouling-resistant Coatings for PWR Fuel Cladding
In Situ EBSD Analysis of Deformation Mechanisms in Highly Irradiated Austenitic Steels
Investigation of the Role of Cr and Cr Carbides at Grain Boundaries in Alloy 600 for Stress Corrosion Cracking
Investigation of Tin as a Fuel Additive to Control FCCI
Investigation on the Damage Mechanism of Plasma-materials Interface by Multi-scale Electron Microscopy Methods
Irradiation Effects on Fe-9%Cr Grain Boundary Strength Measured via In-situ TEM Testing
Irradiation of Additively Manufactured Grade 91 Ferritic/Martensitic Steel
Isothermal Transformation Kinetics of γ phase from α+γ' Phase Mixture in U-10wt.%Mo Alloys
Kinetic Evolution of Transmutation Helium Accumulation at Y-Ti-O Oxides in Nanostructured Ferritic Alloys under Irradiation
Low Cycle Fatigue Resistance of Zircaloy-4 under Uniaxial and Torsion Loading
Mechanical Property Measurements of Zicaloy Hydride Structure by Using Nanoindentation and Nano Mechanical Raman Spectroscopy
Metallurgical Analysis of Ti Addition with Ta in Reduced Activation Ferritic-martensitic Steel
Microstructural and Mechanical Integrity of Laser Weldment of Neutron Irradiated AISI 304 SS
Microstructural Characterization of Plutonium Based Fuels
Microstructural Characterization of U-Mo Fuel Plates Irradiated in the Advanced Test Reactor: Recent Observations
Microstructure Based Hardening Models for Alloys Irradiated with Charged Particles an in the ATR and BOR60 Reactors
Microstructure Evolution in Neutron Irradiated and Ion Irradiated Alloy T91
Multiscale Irradiation Effects of Tungsten Based Materials for Nuclear Power
Neutron irradiation Induced Microstructures in Ferritic/Martensitic Steel HT9
New Insights on Denuded Zone Formation in Polycrystalline Materials
Non-destructive 3D Neutron Imaging of Composition in Nuclear Fuels
Phase Transformation Kinetics in Rolled U-10 wt. % Mo Foil: Effect of Post-rolling Heat Treatment and Prior γ-UMo Grain Size
Phase Verification and Thermophysical Properties of Pu-Zr Alloys
Post-irradiation Examination (PIE) of Irradiated Hafnium
Probing Local Disorder in Ln-UO2 (Ln = Y, Nd, La) and UO2+x Systems
Progress in Developing High Dose Radiation Tolerant Ferritic Steels for Nuclear Applications
Radiation Effect on Nanomaterials at High Temperature -New Type of Radiation Detector for TREAT Nuclear Reactor-
Radiation Effects on HT9 Tempered Martensitic Steels as a Function of Initial Dislocation Density
Radiation Response of Nanoporous Metals
Radiation Tolerance of Equiatomic Multicomponent Single Phase Alloys Subjected to Ion Irradiation at 16 K
Recrystallization of a Nanostructured Ferritic Alloy after Cold Work
Shear Punch Measurement of the Mechanical Properties of Irradiated Cladding Material from ATR Irradiations
The ATR-2 RPV Steel Irradiation Hardening Data Base: An Overview and Some Major Findings
The Effect of Dpa and Dpa Rate on the Strength and Precipitates Stability in Ion-irradiated Inconel 718
The Elastic Constants of γ-phase U – 8 wt% Mo between 25-650°C via Resonant Ultrasound Spectroscopy
Understanding Micromechanical Deformation in Hard-facing Alloys for Improving Galling Resistance
Using Synchrotron X-ray Diffraction and Transmission Electron Microscopy to Study the Dislocation Structures Found in Proton Irradiated Zr-Nb Alloys
Very High Temperature Steam Oxidation of LWR FeCrAl Fuel Cladding
Void Swelling Reduction through Deformation Twinning in Austenitic Stainless Steels

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