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Meeting MS&T22: Materials Science & Technology
Symposium Phase Transformations in Ceramics: Science and Applications
Presentation Title Single Crystal Growth and Characterization of Magnetic Ceramics Using the Laser Heated Pedestal Growth Process
Author(s) Edward Clover Hoffman, Dolendra Karki, Travis Olds, Paul Ohodnicki
On-Site Speaker (Planned) Edward Clover Hoffman
Abstract Scope Single crystal growth of magnetic ceramics will be discussed using laser heated pedestal growth (LHPG). The LHPG method has been adapted as a method for floating zone crystal growth to avoid contamination effects and prompt coherent growth. However, as with any floating zone crystal growth method, there are challenges for growth of homogeneous single crystal oxides which display incongruent melting due to the need to maintain stability of the growth interface and the desire to mitigate compositional segregation within the grown single crystal. In this work we explore feasibility for growth of magnetic ceramics single crystals of stoichiometric chemistry despite modest chemical segregation between the solid and liquid phase predicted at the solidification temperature. Samples prepared through LHPG are characterized using structural and magnetic property characterization methods, and subsequent annealing following single crystal growth is also explored to facilitate chemical homogenization and phase purity of single crystal samples.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Thermodynamic Database for Ultra-high Temperature Ceramics
Crystallization Kinetics of Yttria-doped Ytterbium Disilicate Environmental Barrier Coatings
D-23: Environmental Conical Nozzle Levitator Equipped with Dual Lasers
D-24: Relationship of Bonding Strength with Stability of Ternary Oxide Phases of MgSnO3: A First-principles Study
Far-From-Equilibrium Processing of Materials with Swift Heavy Ions and Mechanical Milling
HfW2O8 and Hf1-xTixW2O8 Negative Thermal Expansion and Phase Transformation
In-situ High Temperature Coefficient of Thermal Expansion of Metal-diborides Through X-ray Diffraction
Martensitic Transformation in Shape Memory Ceramic Composites
Microstructural Evolution of Single Crystal CoTi2O5: A Study Combining Experiment and Simulation
Phase Control of Polytypic Ba0.5Sr0.5MnO3 Films on Polycrystalline Substrates
Phase Stability of Co-substituted Rare Earth Disilicate Systems for Environmental Barrier Coatings
Simulation of ZrO2 Phase Transformation for Superelasticity Understanding
Single Crystal Growth and Characterization of Magnetic Ceramics Using the Laser Heated Pedestal Growth Process
Study Toward Size Dependent Solid State Phase Transition between γ-WO3 and ε-WO3 via In Situ Cryogenic Raman Spectroscopy

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