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Meeting 2021 TMS Annual Meeting & Exhibition
Symposium Mechanical Response of Materials Investigated through Novel In-situ Experiments and Modeling
Presentation Title Advanced In-situ Electrochemical Nanoindentation Testing for Understanding Hydrogen-materials Interactions
Author(s) Verena Maier-Kiener, Anna Ebner, Helmut Clemens, Reinhard Pippan
On-Site Speaker (Planned) Verena Maier-Kiener
Abstract Scope Hydrogen embrittlement mechanisms are still controversially discussed, Especially the role of plasticity itself is often underestimated. Hence, the investigation of deformation processes under hydrogen influence is a broad field of research. In-situ electrochemical nanoindentation became a versatile tool for probing the impact of electrochemical charging on the mechanical properties. Besides measuring hardness and Young’s modulus, deeper insights in the acting deformation mechanisms can be gained by advanced nanoindentation testing methods. The advantages and possibilities of these methods are demonstrated on a precipitation hardened nickel-based alloy. Generally, a hydrogen-induced hardness increase was visible for all applied strain-rates. The measured increase in strain-rate sensitivity and the decrease in activation volume could be related to short range effects, which can lead to a more localized deformation. Furthermore, the evaluation of the remaining imprints with laser scanning confocal microscopy showed a clear change in the evolution of the plastically deformed zone during hydrogen charging.
Proceedings Inclusion? Planned:
Keywords Environmental Effects, Mechanical Properties, Characterization

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Quantitative Assessment of Stress/Strain Partitioning in a Dual-phase Titanium Alloy
Advanced In-situ Electrochemical Nanoindentation Testing for Understanding Hydrogen-materials Interactions
Analysis of Deformation Mechanisms in Advanced FeCrAl Alloy via SEM-EBSD In-situ Testing
Complementary In-situ Methods for Crack Evaluation within High-temperature Materials at Ambient Conditions
Constitutive Model Materials Parameter Determination Using Cyclic Tension-compression Test Data
Creation of Strength Diagrams of Aluminum Flat Products, Dependent on the Different Thermomechanical Processes
Decoupling the Effect of Nanoscale Geometry and Internal Microstructure on the Mechanics of Nanoporous Pt
Deformation Tests of Al Thin Films Using In-situ TEM and Molecular Dynamics Simulations
Dislocation Density Inference from XRD Simulations of In-situ Microstructure Evolution Using Discrete Dislocation Dynamics
Dislocation Pileup Induced Transmission across Grain Boundaries in Aluminum via Molecular Dynamics Simulations
Dislocation Structure in FeCrAl Alloys through Advanced In-situ Microscopy Experiments
Effects of Phase Purity and Pore-reinforcement on the Mechanical Behavior of Metal–organic Frameworks
Experimental Measurements of Anisotropic Mechanical Behavior of 𝛽-HMX Crystals
Giant Superelasticity in SrNi2P2 Micropillars via Lattice Collapse and Expansion
Impact of Precipitate Size, Orientation, and Temperature on Strain Hardening Behavior in Al-Cu Alloys
In-situ Analysis of Powder Bed Quality during Selective Laser Melting
In-situ Characterization of Material under Extreme Thermal Cycling Using High-speed Synchrotron X-ray Diffraction
In-situ Characterization of the Damage Initiation and Evolution in Sustainable Cellulose-based Cottonid
In-situ Experimental Evaluation of Residual Stresses in Composites during Autoclave Manufacturing
In-situ Investigation of Intergranular Crack Initiation in Hydrogen Embrittled Inconel 725
In-situ Micro-tensile Testing of Proton-irradiated HT-9 Steels
In-situ Nanomechanics of Ni-based Superalloys and Bond Coating at Room Temperature to 1000C
In-situ TEM Investigation of the Electroplasticity Phenomenon in Ti-6Al
In-situ X-Ray Diffraction Investigation of High-strain Rate, High-temperature Deformation in Microalloyed Steel
Low Temperature Failure Mechanism of [001] Niobium Micropillars under Uniaxial Tension
Mechanical Behavior and Microstructural Evolution of a Cu-0.7Cr-0.1Zr Alloy at Cryogenic Temperature: An In-situ Synchrotron X-ray Evaluation
MEMS-based In-situ Tensile Experiments Designed to Arrest Catastrophic Failure in Brittle Nanomaterials
Metal Foams: Linking Dynamic CT Results to Simulation and Modeling
Microscale Insight into the Effect of Twinning on Fracture in a Manganese Steel
Microstructural Anisotropy and Its Influence on the Internal Stress Field within Grains: Experimental Confrontation with Full Field Crystal Plasticity Models
Microstructural Influences on Grain Boundary Sliding in High Purity Aluminum
Multiphysics Modeling of Coupled Chemical-Thermal-mechanical Phenomena in Chemically Blown Polyurethane Foams during Manufacturing
Non-destructive Inspection of Contaminated Epoxy Plates Using Propagating Acoustic Waves
Non-linear Reversible Behaviour of Metallic Alloys at Low Stresses
Observation of Microstructure Evolution in Pure Copper and Copper-8 wt. % Aluminium Alloy during Deformation
Quantifying Electron Beam Effects during In-situ TEM Nanomechanical Tensile Testing on Aluminum Thin Films
Quantifying the Long-range Stress ahead of the Tip of a Dislocation Pileup at a Grain Boundary and Its Contribution to the Subsequent Structure Changes in Ti-alloys from the Atomistic to the Mesoscale
Rhodium and Cobalt Oxidation: A Nanoscale Study by In-situ and in Operando Atom Probe Tomography
Ripplocations: A Novel Deformation Mechanism in Layered Crystalline Solids
Size Effects in Barium Titanate
Size Effect, Friction and Adhesion in Small-scale Cutting of Metals
Sub-surface Microtensile Testing in Oxidized Equiatomic Alloy NbTiCr
Surface Erosion of Spacecraft by High-velocity Regolith Impacts to Simulate Wind Storms on Martian Surfaces
Synchrotron X-ray Studies of Deformation and Failure in Cold Spray Composites
The Effect of Material Volume on Impact Energy Absorption for Protective Equipment Applications

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